Separation of D-amino acids by capillary electrophoresis using P-aectamidobenzenesulfonyl fluoride as derivatization reagent

	Separation of D-amino acids by capillary electrophoresis using P-aectamidobenzenesulfonyl fluoride as derivatization reagent
	Qu Qishu ; Tang Xiaoqing ; Wang Chengyin ; Yang Gongjun ; Hu Xiaoya ; Zhang Yukui ; Yan Chao
刊名	chinese journal of analytical chemistry
	2006-11-01
卷号	34 期号:11 页码:1587-1590
关键词	capillary electrophoresis D-amino acid derivatization
英文摘要	a new method for the separation of 19 standard d-amino acids and glycine ( gly) by capillary electrophoresis ( ce) using p-acetamidobenzenesulfonyl fluoride ( paabs-f) as precolumn derivatization reagent has been developed. the separation conditions were carefully studied and optimized. the experimental results showed that 20 mmmol/l sodium borate ( ph 9.3), 126 mmmol/l sodium dodecyl sulfate, 8 mmol/l,8-cyclodextrin and 20 mmol/l nacl were the optimal conditions for the ce separation. under the optimal conditions, 19 stangdard d-amino acids and gly were successfully achied with baseline separation within 16 min by ce.
WOS标题词	science & technology ; physical sciences
类目[WOS]	chemistry, analytical
研究领域[WOS]	chemistry
关键词[WOS]	chromatography
收录类别	SCI
语种	英语
WOS记录号	WOS:000244672100016
公开日期	2015-11-17
内容类型	期刊论文
源URL	[http://159.226.238.44/handle/321008/140251]
专题	大连化学物理研究所_中国科学院大连化学物理研究所
作者单位	1.Yangzhou Univ, Jiangsu Key Lab Environm Mat & Environm Engn, Coll Chem & Chem Engn, Yangzhou 225002, Peoples R China 2.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog Res & Anal Ctr, Dalian 116011, Peoples R China
推荐引用方式 GB/T 7714	Qu Qishu,Tang Xiaoqing,Wang Chengyin,et al. Separation of D-amino acids by capillary electrophoresis using P-aectamidobenzenesulfonyl fluoride as derivatization reagent[J]. chinese journal of analytical chemistry,2006,34(11):1587-1590.
APA	Qu Qishu.,Tang Xiaoqing.,Wang Chengyin.,Yang Gongjun.,Hu Xiaoya.,...&Yan Chao.(2006).Separation of D-amino acids by capillary electrophoresis using P-aectamidobenzenesulfonyl fluoride as derivatization reagent.chinese journal of analytical chemistry,34(11),1587-1590.
MLA	Qu Qishu,et al."Separation of D-amino acids by capillary electrophoresis using P-aectamidobenzenesulfonyl fluoride as derivatization reagent".chinese journal of analytical chemistry 34.11(2006):1587-1590.