Pulse Electric Current- Aided Reactive Sintering of High- Purity Zr3Al3C5

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	Pulse Electric Current- Aided Reactive Sintering of High- Purity Zr3Al3C5
	Zhou, Jie ; Qiu, Fagui ; Shen, Lu ; Li, Fangzhi ; Xue, Jianming ; Barsoum, Michel W. ; Huang, Qing
刊名	JOURNAL OF THE AMERICAN CERAMIC SOCIETY
	2014
卷号	97 期号:4 页码:1296
中文摘要	Herein, we report on the in situ reactive synthesis and simultaneous densification of a high-purity ternary Zr3Al3C5 phase via pulse electric current sintering (PECS) of Zr/Al/graphite powder mixtures with a molar ratio of 3:3.2:4.8. The phases and microstructure evolution in the 580 degrees C-1800 degrees C temperature range were characterized by X-ray diffraction, real-time sintering curves, and a scanning electron microscope equipped with an energy dispersive spectroscope. An additive-free, fully dense Zr3Al3C5 compound was obtained at 1800 degrees C using a load corresponding to a stress of 35MPa for 20min. The final product was comprised of 96.61wt% Zr3Al3C5, 3.14wt% ZrC, and 0.25wt% Zr2Al3C4; the relative density was 97%.
公开日期	2015-09-20
内容类型	期刊论文
源URL	[http://ir.nimte.ac.cn/handle/174433/11887]
专题	宁波材料技术与工程研究所_2014专题
推荐引用方式 GB/T 7714	Zhou, Jie,Qiu, Fagui,Shen, Lu,et al. Pulse Electric Current- Aided Reactive Sintering of High- Purity Zr3Al3C5[J]. JOURNAL OF THE AMERICAN CERAMIC SOCIETY,2014,97(4):1296.
APA	Zhou, Jie.,Qiu, Fagui.,Shen, Lu.,Li, Fangzhi.,Xue, Jianming.,...&Huang, Qing.(2014).Pulse Electric Current- Aided Reactive Sintering of High- Purity Zr3Al3C5.JOURNAL OF THE AMERICAN CERAMIC SOCIETY,97(4),1296.
MLA	Zhou, Jie,et al."Pulse Electric Current- Aided Reactive Sintering of High- Purity Zr3Al3C5".JOURNAL OF THE AMERICAN CERAMIC SOCIETY 97.4(2014):1296.