Solvothermal synthesis of nanosized TiO2 particles with different crystal structures and their photocatalytic activities
Qin Wei ; Liu Jian-Jun ; Zuo Sheng-Li ; Yu Ying-Chun ; Hao Zheng-Ping
刊名JOURNAL OF INORGANIC MATERIALS
2007-09
卷号22期号:5页码:931-936
关键词solvothermal synthesis titania phase composition photocatalysis
英文摘要Nanosized titania particles consisting of anatase, rutile and brookite phases were synthesized under solvothermal conditions with different alcohols as solvents, hexamethylene tetramine (HMT) as precipitant as well as precursor of titanium trichloride. XRD, TEM, UV-Vis and XPS spectra were employed to characterize these samples. The effect of treatment solvent and HMT amount on the phase composition and photocatalytic activity of titania were investigated. It is found that anatase is easier to form at acidic condition, but rutile and brookite at basic condition, using methanol as solvent. The TiO2-N-x(x) with nitrogen doping in TiO2 is obtained under solvothermal conditions. The results of photocatalytic degradation to methyl orange show that the mixed crystallite of anatase and brookite has the best photocatalytic activity.
WOS记录号WOS:000249771300031
内容类型期刊论文
源URL[http://ir.rcees.ac.cn/handle/311016/22527]  
专题生态环境研究中心_环境纳米材料实验室
推荐引用方式
GB/T 7714
Qin Wei,Liu Jian-Jun,Zuo Sheng-Li,et al. Solvothermal synthesis of nanosized TiO2 particles with different crystal structures and their photocatalytic activities[J]. JOURNAL OF INORGANIC MATERIALS,2007,22(5):931-936.
APA Qin Wei,Liu Jian-Jun,Zuo Sheng-Li,Yu Ying-Chun,&Hao Zheng-Ping.(2007).Solvothermal synthesis of nanosized TiO2 particles with different crystal structures and their photocatalytic activities.JOURNAL OF INORGANIC MATERIALS,22(5),931-936.
MLA Qin Wei,et al."Solvothermal synthesis of nanosized TiO2 particles with different crystal structures and their photocatalytic activities".JOURNAL OF INORGANIC MATERIALS 22.5(2007):931-936.
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