Trace Analysis of Fifteen Androgens in Environmental Waters by LC-ESI-MS-MS Combined with Solid-Phase Disk Extraction Cleanup

CORC > 生态环境研究中心 > 中国科学院生态环境研究中心 > 环境化学与生态毒理学国家重点实验室

	Trace Analysis of Fifteen Androgens in Environmental Waters by LC-ESI-MS-MS Combined with Solid-Phase Disk Extraction Cleanup
	Sun, Li; Liu, Yan; Chu, Xiaogan; Lin, Jin-Ming
刊名	CHROMATOGRAPHIA
	2010-05
卷号	71 期号:3 页码:867-873
关键词	Column liquid chromatography ESI-MS-MS Solid-phase disk extraction Environmental water Androgens
中文摘要	A rapid and sensitive liquid chromatography-electrospray tandem mass spectrometry method, combined with solid-phase disk extraction cleanup, was developed and applied to the analysis of fifteen androgens in waste water. Compounds included androstenedione, androstanolone, boldenone, clostebol, danazol, 6-dehydronandrolone acetate, fluoxymesterone, methyltestosterone, nandrolone, nandrolone propionate, testosterone, testosterone acetate, testosterone propionate, trenbolone and trenbolone acetate, respectively. The overall method recoveries ranged from 78.0 to 107.7% and the limits of detection for the fifteen analytes determined in influent samples were between 0.5 and 4 ng L(-1). The analysis of residual androgens was carried out in waste water obtained from the Beijing area and five analytes (androstenedione, fluoxymesterone, methyltestosterone, testosterone and nandrolone) could be detected in levels ranging from 1.6-3.5, 7.6-66.7, 4.1-7.0, 1.2-4.3 and 1.7 ng L(-1), respectively.
WOS记录号	WOS:000277595400017
内容类型	期刊论文
源URL	[http://ir.rcees.ac.cn/handle/311016/21163]
专题	生态环境研究中心_环境化学与生态毒理学国家重点实验室
推荐引用方式 GB/T 7714	Sun, Li,Liu, Yan,Chu, Xiaogan,et al. Trace Analysis of Fifteen Androgens in Environmental Waters by LC-ESI-MS-MS Combined with Solid-Phase Disk Extraction Cleanup[J]. CHROMATOGRAPHIA,2010,71(3):867-873.
APA	Sun, Li,Liu, Yan,Chu, Xiaogan,&Lin, Jin-Ming.(2010).Trace Analysis of Fifteen Androgens in Environmental Waters by LC-ESI-MS-MS Combined with Solid-Phase Disk Extraction Cleanup.CHROMATOGRAPHIA,71(3),867-873.
MLA	Sun, Li,et al."Trace Analysis of Fifteen Androgens in Environmental Waters by LC-ESI-MS-MS Combined with Solid-Phase Disk Extraction Cleanup".CHROMATOGRAPHIA 71.3(2010):867-873.