Distance measurement between a spin-1/2 and a half-integer quadrupolar nuclei by solid-state NMR using exact analytical expressions

CORC > 武汉物理与数学研究所 > 中国科学院武汉物理与数学研究所 > 2011年以前论文发表（包括2011年）

	Distance measurement between a spin-1/2 and a half-integer quadrupolar nuclei by solid-state NMR using exact analytical expressions
	Chen, Lei 1; Lu, Xingyu 2; Wang, Qiang 1,2,3; Lafon, Olivier 2; Trebosc, Julien 2; Deng, Feng 1; Amoureux, Jean-Paul 2
刊名	JOURNAL OF MAGNETIC RESONANCE
	2010-10-01
卷号	206 期号:2 页码:269-273
关键词	Solid-state NMR Quadrupolar nuclei Distance measurement Saturation pulse
产权排序	第一
英文摘要	We show that the S-RESPDOR NMR method can be used to measure distances between spin-1/2 and half-integer quadrupolar nuclei, and that a general analytical formula describes its dephasing curve for all spin values. We demonstrate the method on the C(4)-O(4) spin pair of t-tyrosine. HCl, with (13)C natural abundance and 30% (17)O enrichment, using a moderate magnetic field (9.4 T), a moderate (17)O rf-field (40 kHz) and a fast spinning speed (22 kHz). It is shown that S-RESPDOR is much more robust and accurate than previous methods. (C) 2010 Elsevier Inc. All rights reserved.
学科主题	波谱分析
WOS标题词	Science & Technology ; Life Sciences & Biomedicine ; Physical Sciences ; Technology
类目[WOS]	Biochemical Research Methods ; Physics, Atomic, Molecular & Chemical ; Spectroscopy
研究领域[WOS]	Biochemistry & Molecular Biology ; Physics ; Spectroscopy
关键词[WOS]	DOUBLE-RESONANCE NMR ; ECHO DOUBLE-RESONANCE ; CHEMICAL-SHIFT CORRELATION ; INDUCED DIPOLAR EXCHANGE ; ANGLE-SPINNING NMR ; ROTATIONAL-ECHO ; THROUGH-BOND ; CORRELATION SPECTROSCOPY ; ADIABATIC-PASSAGE ; REAPDOR NMR
收录类别	SCI
语种	英语
WOS记录号	WOS:000282196900012
内容类型	期刊论文
源URL	[http://ir.wipm.ac.cn/handle/112942/2030]
专题	武汉物理与数学研究所_2011年以前论文发表（包括2011年）
作者单位	1.Chinese Acad Sci, Wuhan Inst Phys & Math, Wuhan Ctr Magnet Resonance, State Key Lab Magnet Resonance & Atom & Mol Phys, Wuhan 430071, Peoples R China 2.Lille N France Univ, CNRS 8181, Unit Catalysis & Chem Solids, F-59652 Lille, France 3.Chinese Acad Sci, Grad Sch, Beijing, Peoples R China
推荐引用方式 GB/T 7714	Chen, Lei,Lu, Xingyu,Wang, Qiang,et al. Distance measurement between a spin-1/2 and a half-integer quadrupolar nuclei by solid-state NMR using exact analytical expressions[J]. JOURNAL OF MAGNETIC RESONANCE,2010,206(2):269-273.
APA	Chen, Lei.,Lu, Xingyu.,Wang, Qiang.,Lafon, Olivier.,Trebosc, Julien.,...&Amoureux, Jean-Paul.(2010).Distance measurement between a spin-1/2 and a half-integer quadrupolar nuclei by solid-state NMR using exact analytical expressions.JOURNAL OF MAGNETIC RESONANCE,206(2),269-273.
MLA	Chen, Lei,et al."Distance measurement between a spin-1/2 and a half-integer quadrupolar nuclei by solid-state NMR using exact analytical expressions".JOURNAL OF MAGNETIC RESONANCE 206.2(2010):269-273.