Comparative Determination of the Volatile Components of Prunella vulgaris L. from Different Geographical Origins by Headspace Solid-Phase Microextraction and Gas Chromatography-Mass Spectrometry | |
Yang YQ ; Nan HM ; Wang GH ; Yang W ; Xu JW | |
刊名 | analytical letters |
2013 | |
卷号 | 46期号:13页码:2001-2016 |
关键词 | ESSENTIAL OILS GC-MS CONVENTIONAL EXTRACTION SUPERCRITICAL-FLUID VAR. LILACINA IN-VITRO LEAVES CELLS MICE CONSTITUENTS |
ISSN号 | 0003-2719 |
通讯作者 | xu jw |
中文摘要 | the volatile components of prunella vulgaris l. were determined by headspace solid-phase microextraction (hs-spme) combined with gas chromatography-mass spectrometry (gc-ms). the optimal conditions for hs-spme were 1.5g of sample, extraction using a polydimethylsiloxane-divinylbenzene fiber for 50min at 90 degrees c, and a desorption time of 5min. the volatile compounds of prunella vulgaris l. from different parts of the herb (cultivated in jiangsu) and from different geographical regions (jiangsu, fujian, guangxi, hunan, and zhejiang) were comparatively analyzed. there were 26, 28, 28, 28, and 34 compounds identified in prunella vulgaris l. from jiangsu, fujian, guangxi, hunan, and zhejiang, respectively. among them, the following 12 were found in all origins: 1-nonanol, dodecane, tridecane, -bourbonene, tetradecane, geranyl acetone, pentadecane, caryophyllene oxide, hexadecane, tetradecanal, isobutyl phthalate, and n-butyl hexadecanoate. in addition, prunella vulgaris l. cultivated in guangxi and zhejiang had a high similarity in volatile components as did prunella vulgaris l. cultivated in fujian and hunan. the results provided valuable information for the application of prunella vulgaris l. and suggested that the hs-spme method was suitable for differentiating and determining the volatile components of prunella vulgaris l. |
收录类别 | SCI收录期刊论文 |
语种 | 英语 |
WOS记录号 | WOS:000323475300002 |
公开日期 | 2014-04-15 |
内容类型 | 期刊论文 |
源URL | [http://ir.ciac.jl.cn/handle/322003/49631] |
专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
推荐引用方式 GB/T 7714 | Yang YQ,Nan HM,Wang GH,et al. Comparative Determination of the Volatile Components of Prunella vulgaris L. from Different Geographical Origins by Headspace Solid-Phase Microextraction and Gas Chromatography-Mass Spectrometry[J]. analytical letters,2013,46(13):2001-2016. |
APA | Yang YQ,Nan HM,Wang GH,Yang W,&Xu JW.(2013).Comparative Determination of the Volatile Components of Prunella vulgaris L. from Different Geographical Origins by Headspace Solid-Phase Microextraction and Gas Chromatography-Mass Spectrometry.analytical letters,46(13),2001-2016. |
MLA | Yang YQ,et al."Comparative Determination of the Volatile Components of Prunella vulgaris L. from Different Geographical Origins by Headspace Solid-Phase Microextraction and Gas Chromatography-Mass Spectrometry".analytical letters 46.13(2013):2001-2016. |
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