Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions | |
Zhao, Xinhong1; Zhao, Jiangbo1; Wen, Juanjuan1; Li, An1; Li, Guixian1; Wang, Xiaolai2 | |
刊名 | MICROPOROUS AND MESOPOROUS MATERIALS
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2015-09 | |
卷号 | 213页码:192-196 |
关键词 | AlPO4-5 Solvent-free Hierarchical porous Microwave |
ISSN号 | 1387-1811 |
DOI | 10.1016/j.micromeso.2015.03.031 |
英文摘要 | AlPO4-5 aluminophosphate molecular sieve with AFT topology has been successfully synthesized by microwave irradiation under solvent-free conditions. The key influential factors controlling the crystallization of AFI structure were thoroughly investigated. The optimum synthetic conditions of this material are as follows: the initial composition is 1.0Al(2)O(3): 3.0P(2)O(5): 2.0HF: 8.0TEABr(tetraethylammonium bromide): 125C, aluminum isopropoxide is the best aluminum source, and activated carbon needs to be pretreated before used as the reaction medium and hard template. The resultant AlPO4-5 molecular sieves were characterized by X-ray diffraction (XRD), N-2 physisorption, scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The results reveal that the obtained samples exhibit hierarchically porous characteristic. (C) 2015 Elsevier Inc. All rights reserved. |
资助项目 | Development Program of Lanzhou University of Technology for excellent teachers[Q201113] |
WOS研究方向 | Chemistry ; Science & Technology - Other Topics ; Materials Science |
语种 | 英语 |
出版者 | ELSEVIER SCIENCE BV |
WOS记录号 | WOS:000356186900024 |
状态 | 已发表 |
内容类型 | 期刊论文 |
源URL | [http://119.78.100.223/handle/2XXMBERH/33991] ![]() |
专题 | 石油化工学院 |
通讯作者 | Zhao, Xinhong |
作者单位 | 1.Lanzhou Univ Technol, Sch Petrochem Engn, Lanzhou 730050, Peoples R China 2.Chinese Acad Sci, Lanzhou Inst Chem Phys, State Key Lab Oxo Synth & Select Oxidat, Lanzhou 730000, Peoples R China |
推荐引用方式 GB/T 7714 | Zhao, Xinhong,Zhao, Jiangbo,Wen, Juanjuan,et al. Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions[J]. MICROPOROUS AND MESOPOROUS MATERIALS,2015,213:192-196. |
APA | Zhao, Xinhong,Zhao, Jiangbo,Wen, Juanjuan,Li, An,Li, Guixian,&Wang, Xiaolai.(2015).Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions.MICROPOROUS AND MESOPOROUS MATERIALS,213,192-196. |
MLA | Zhao, Xinhong,et al."Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions".MICROPOROUS AND MESOPOROUS MATERIALS 213(2015):192-196. |
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