Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions

doi:10.1016/j.micromeso.2015.03.031

CORC > 兰州理工大学 > 兰州理工大学 > 石油化工学院

	Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions
	Zhao, Xinhong 1; Zhao, Jiangbo 1; Wen, Juanjuan 1; Li, An 1; Li, Guixian 1; Wang, Xiaolai 2
刊名	MICROPOROUS AND MESOPOROUS MATERIALS
	2015-09
卷号	213 页码:192-196
关键词	AlPO4-5 Solvent-free Hierarchical porous Microwave
ISSN号	1387-1811
DOI	10.1016/j.micromeso.2015.03.031
英文摘要	AlPO4-5 aluminophosphate molecular sieve with AFT topology has been successfully synthesized by microwave irradiation under solvent-free conditions. The key influential factors controlling the crystallization of AFI structure were thoroughly investigated. The optimum synthetic conditions of this material are as follows: the initial composition is 1.0Al(2)O(3): 3.0P(2)O(5): 2.0HF: 8.0TEABr(tetraethylammonium bromide): 125C, aluminum isopropoxide is the best aluminum source, and activated carbon needs to be pretreated before used as the reaction medium and hard template. The resultant AlPO4-5 molecular sieves were characterized by X-ray diffraction (XRD), N-2 physisorption, scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The results reveal that the obtained samples exhibit hierarchically porous characteristic. (C) 2015 Elsevier Inc. All rights reserved.
资助项目	Development Program of Lanzhou University of Technology for excellent teachers[Q201113]
WOS研究方向	Chemistry ; Science & Technology - Other Topics ; Materials Science
语种	英语
出版者	ELSEVIER SCIENCE BV
WOS记录号	WOS:000356186900024
状态	已发表
内容类型	期刊论文
源URL	[http://119.78.100.223/handle/2XXMBERH/33991]
专题	石油化工学院
通讯作者	Zhao, Xinhong
作者单位	1.Lanzhou Univ Technol, Sch Petrochem Engn, Lanzhou 730050, Peoples R China 2.Chinese Acad Sci, Lanzhou Inst Chem Phys, State Key Lab Oxo Synth & Select Oxidat, Lanzhou 730000, Peoples R China
推荐引用方式 GB/T 7714	Zhao, Xinhong,Zhao, Jiangbo,Wen, Juanjuan,et al. Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions[J]. MICROPOROUS AND MESOPOROUS MATERIALS,2015,213:192-196.
APA	Zhao, Xinhong,Zhao, Jiangbo,Wen, Juanjuan,Li, An,Li, Guixian,&Wang, Xiaolai.(2015).Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions.MICROPOROUS AND MESOPOROUS MATERIALS,213,192-196.
MLA	Zhao, Xinhong,et al."Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions".MICROPOROUS AND MESOPOROUS MATERIALS 213(2015):192-196.