Influence of Compaction Pressure on Particle Size and Purity of Ultra-fine CeB6 powders Prepared by Salt-assisted Combustion Synthesis and Its Mechanism
Wang Qianlong; Ou Yujing; La Peiqing; Feng Jing; Li Zhengning; Shi Yu
刊名RARE METAL MATERIALS AND ENGINEERING
2019-02
卷号48期号:2页码:662-667
关键词salt-assisted combustion molding pressure CeB6 powder average particle size
ISSN号1002-185X
英文摘要The exothermal agent KClO3 was added to the B2O3-CeO2-Mg system to prepare the ultra-fine CeB6 powders via salt-assisted combustion synthesis. The products were analyzed by XRD, SEM, EDS and TEM. The formation mechanisms of the CeB6 as well as the effect of compaction pressure on the phase composition, average particle size and purity of the products after leaching were studied. Results show that the main product of combustion synthesis is CeB6. With increasing the compaction pressure, the average particle size of the synthesis products increases slightly after leaching, which is 0.830-0.930 mu m and the particle size distribution of powders is uniform. However, the purity of CeB6 reaches a maximum of 99.0 wt% when the pressure is 20 MPa. The purity of all products under different pressures exceeds 98.0%.
WOS研究方向Materials Science ; Metallurgy & Metallurgical Engineering
语种中文
出版者NORTHWEST INST NONFERROUS METAL RESEARCH
WOS记录号WOS:000460987600044
状态已发表
内容类型期刊论文
源URL[http://119.78.100.223/handle/2XXMBERH/32107]  
专题省部共建有色金属先进加工与再利用国家重点实验室
材料科学与工程学院
石油化工学院
通讯作者La Peiqing
作者单位Lanzhou Univ Technol, State Key Lab Adv Proc & Recycling Nonferrous Met, Lanzhou 730050, Gansu, Peoples R China
推荐引用方式
GB/T 7714
Wang Qianlong,Ou Yujing,La Peiqing,et al. Influence of Compaction Pressure on Particle Size and Purity of Ultra-fine CeB6 powders Prepared by Salt-assisted Combustion Synthesis and Its Mechanism[J]. RARE METAL MATERIALS AND ENGINEERING,2019,48(2):662-667.
APA Wang Qianlong,Ou Yujing,La Peiqing,Feng Jing,Li Zhengning,&Shi Yu.(2019).Influence of Compaction Pressure on Particle Size and Purity of Ultra-fine CeB6 powders Prepared by Salt-assisted Combustion Synthesis and Its Mechanism.RARE METAL MATERIALS AND ENGINEERING,48(2),662-667.
MLA Wang Qianlong,et al."Influence of Compaction Pressure on Particle Size and Purity of Ultra-fine CeB6 powders Prepared by Salt-assisted Combustion Synthesis and Its Mechanism".RARE METAL MATERIALS AND ENGINEERING 48.2(2019):662-667.
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