Influence of Compaction Pressure on Particle Size and Purity of Ultra-fine CeB6 powders Prepared by Salt-assisted Combustion Synthesis and Its Mechanism | |
Wang Qianlong; Ou Yujing; La Peiqing; Feng Jing; Li Zhengning; Shi Yu | |
刊名 | RARE METAL MATERIALS AND ENGINEERING |
2019-02 | |
卷号 | 48期号:2页码:662-667 |
关键词 | salt-assisted combustion molding pressure CeB6 powder average particle size |
ISSN号 | 1002-185X |
英文摘要 | The exothermal agent KClO3 was added to the B2O3-CeO2-Mg system to prepare the ultra-fine CeB6 powders via salt-assisted combustion synthesis. The products were analyzed by XRD, SEM, EDS and TEM. The formation mechanisms of the CeB6 as well as the effect of compaction pressure on the phase composition, average particle size and purity of the products after leaching were studied. Results show that the main product of combustion synthesis is CeB6. With increasing the compaction pressure, the average particle size of the synthesis products increases slightly after leaching, which is 0.830-0.930 mu m and the particle size distribution of powders is uniform. However, the purity of CeB6 reaches a maximum of 99.0 wt% when the pressure is 20 MPa. The purity of all products under different pressures exceeds 98.0%. |
WOS研究方向 | Materials Science ; Metallurgy & Metallurgical Engineering |
语种 | 中文 |
出版者 | NORTHWEST INST NONFERROUS METAL RESEARCH |
WOS记录号 | WOS:000460987600044 |
状态 | 已发表 |
内容类型 | 期刊论文 |
源URL | [http://119.78.100.223/handle/2XXMBERH/32107] |
专题 | 省部共建有色金属先进加工与再利用国家重点实验室 材料科学与工程学院 石油化工学院 |
通讯作者 | La Peiqing |
作者单位 | Lanzhou Univ Technol, State Key Lab Adv Proc & Recycling Nonferrous Met, Lanzhou 730050, Gansu, Peoples R China |
推荐引用方式 GB/T 7714 | Wang Qianlong,Ou Yujing,La Peiqing,et al. Influence of Compaction Pressure on Particle Size and Purity of Ultra-fine CeB6 powders Prepared by Salt-assisted Combustion Synthesis and Its Mechanism[J]. RARE METAL MATERIALS AND ENGINEERING,2019,48(2):662-667. |
APA | Wang Qianlong,Ou Yujing,La Peiqing,Feng Jing,Li Zhengning,&Shi Yu.(2019).Influence of Compaction Pressure on Particle Size and Purity of Ultra-fine CeB6 powders Prepared by Salt-assisted Combustion Synthesis and Its Mechanism.RARE METAL MATERIALS AND ENGINEERING,48(2),662-667. |
MLA | Wang Qianlong,et al."Influence of Compaction Pressure on Particle Size and Purity of Ultra-fine CeB6 powders Prepared by Salt-assisted Combustion Synthesis and Its Mechanism".RARE METAL MATERIALS AND ENGINEERING 48.2(2019):662-667. |
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