Synthesis of amino-silane modified magnetic silica adsorbents and application for adsorption of flavonoids from Glycyrrhiza uralensis Fisch
Zhang Bo1,2; Xing JianMin1; Lang YuQi1,2; Liu HuiZhou1
刊名SCIENCE IN CHINA SERIES B-CHEMISTRY
2008-02-01
卷号51期号:2页码:145-151
关键词magnetic adsorbents flavonoids Glycyrrhiza uralensis Fisch
ISSN号1006-9291
其他题名Sci. China Ser. B-Chem.
中文摘要Magnetic separation technology was applied in the separation of flavonoids from the licorice root in this work. Licorice flavonoids (LF) displayed a remarkable array of biological and pharmacological activities. The magnetic adsorbents with functional -NH(2) groups were synthesized by immobilization of amino-silane on the surface of the magnetic silica supports, which were prepared by co-precipitation method. The adsorption and desorption characteristics of the magnetic adsorbents for the separation of LF have been evaluated. The purity of an enriched extract with this method was 16.7% while the crude extract only had about 6.8% purity. Therefore, it can be concluded that these kinds of magnetic adsorbents have selectivity to the flavonoids to some extent. The affinity selectivity of the adsorbents is based on the formation of hydrogen bonding between the -NH(2) on the magnetic adsorbents and -OH, -CO on the flavonoids.
英文摘要Magnetic separation technology was applied in the separation of flavonoids from the licorice root in this work. Licorice flavonoids (LF) displayed a remarkable array of biological and pharmacological activities. The magnetic adsorbents with functional -NH(2) groups were synthesized by immobilization of amino-silane on the surface of the magnetic silica supports, which were prepared by co-precipitation method. The adsorption and desorption characteristics of the magnetic adsorbents for the separation of LF have been evaluated. The purity of an enriched extract with this method was 16.7% while the crude extract only had about 6.8% purity. Therefore, it can be concluded that these kinds of magnetic adsorbents have selectivity to the flavonoids to some extent. The affinity selectivity of the adsorbents is based on the formation of hydrogen bonding between the -NH(2) on the magnetic adsorbents and -OH, -CO on the flavonoids.
WOS标题词Science & Technology ; Physical Sciences
类目[WOS]Chemistry, Multidisciplinary
研究领域[WOS]Chemistry
关键词[WOS]LICORICE ; NANOPARTICLES ; SEPARATION ; CONSTITUENTS ; EXTRACTS ; CELLS
收录类别SCI
原文出处://WOS:000252470300007
语种英语
WOS记录号WOS:000252470300007
公开日期2013-10-08
内容类型期刊论文
版本出版稿
源URL[http://ir.ipe.ac.cn/handle/122111/2903]  
专题过程工程研究所_研究所(批量导入)
作者单位1.Chinese Acad Sci, Inst Proc Engn, Lab Separat Sci & Engn, Beijing 100080, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China
推荐引用方式
GB/T 7714
Zhang Bo,Xing JianMin,Lang YuQi,et al. Synthesis of amino-silane modified magnetic silica adsorbents and application for adsorption of flavonoids from Glycyrrhiza uralensis Fisch[J]. SCIENCE IN CHINA SERIES B-CHEMISTRY,2008,51(2):145-151.
APA Zhang Bo,Xing JianMin,Lang YuQi,&Liu HuiZhou.(2008).Synthesis of amino-silane modified magnetic silica adsorbents and application for adsorption of flavonoids from Glycyrrhiza uralensis Fisch.SCIENCE IN CHINA SERIES B-CHEMISTRY,51(2),145-151.
MLA Zhang Bo,et al."Synthesis of amino-silane modified magnetic silica adsorbents and application for adsorption of flavonoids from Glycyrrhiza uralensis Fisch".SCIENCE IN CHINA SERIES B-CHEMISTRY 51.2(2008):145-151.
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