Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235) | |
Sun, Z. D.1,2,3; Yang, Y. N.2; Li, Q. K.1; Liu, J. G.1; Xu, Q.2,4; Yan, C. W.1 | |
刊名 | MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK |
2020-04-01 | |
卷号 | 51期号:4页码:480-487 |
关键词 | Epoxy resin silane treatment orthogonal test adhesion Q235 steel |
ISSN号 | 0933-5137 |
DOI | 10.1002/mawe.201900150 |
通讯作者 | Sun, Z. D.(sunzd@sie.edu.cn) |
英文摘要 | In this investigation, the mixed gamma-GPS/BTSE silane solution for preparing well adhered composite gamma-GPS/BTSE silane film on Q235 carbon steel surface has been successfully optimized by orthogonal test, and the curing process parameters of temperature and time have also been optimized. The results indicate that the optimized hydrolysis parameters for mixed silanes agent solution are as follows: V-ethanol/V-water 3 : 1, V gamma-GPS/V-BTSE 2 : 3, V-silanes 6 vol.%, pH 4.0 and hydrolysis time 72 h. In addition, the optimized curing condition for composite gamma-GPS/BTSE silane film is 120 degrees C and 30 min. After immersion in the optimized mixed gamma-GPS/BTSE silanes agent solution and curing under the optimized condition, the prepared composite gamma-GPS/BTSE silane film on Q235 steel surface can have an adhesion strength of 24.52 MPa to underlying steel substrate. |
WOS研究方向 | Materials Science |
语种 | 英语 |
出版者 | WILEY-V C H VERLAG GMBH |
WOS记录号 | WOS:000525608800008 |
内容类型 | 期刊论文 |
源URL | [http://ir.imr.ac.cn/handle/321006/138355] |
专题 | 金属研究所_中国科学院金属研究所 |
通讯作者 | Sun, Z. D. |
作者单位 | 1.Chinese Acad Sci, Inst Met Res, Lab Corros & Protect Met, Shenyang 110016, Peoples R China 2.Northeastern Univ, Sch Met, Shenyang 110819, Peoples R China 3.Shenyang Inst Engn, Shenyang 110136, Peoples R China 4.Shanghai Univ, Sch Mat Sci & Engn, State Key Lab Adv Special Steel, Shanghai 200072, Peoples R China |
推荐引用方式 GB/T 7714 | Sun, Z. D.,Yang, Y. N.,Li, Q. K.,et al. Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235)[J]. MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK,2020,51(4):480-487. |
APA | Sun, Z. D.,Yang, Y. N.,Li, Q. K.,Liu, J. G.,Xu, Q.,&Yan, C. W..(2020).Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235).MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK,51(4),480-487. |
MLA | Sun, Z. D.,et al."Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235)".MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK 51.4(2020):480-487. |
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