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Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235)
Sun, Z. D.1,2,3; Yang, Y. N.2; Li, Q. K.1; Liu, J. G.1; Xu, Q.2,4; Yan, C. W.1
刊名MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK
2020-04-01
卷号51期号:4页码:480-487
关键词Epoxy resin silane treatment orthogonal test adhesion Q235 steel
ISSN号0933-5137
DOI10.1002/mawe.201900150
通讯作者Sun, Z. D.(sunzd@sie.edu.cn)
英文摘要In this investigation, the mixed gamma-GPS/BTSE silane solution for preparing well adhered composite gamma-GPS/BTSE silane film on Q235 carbon steel surface has been successfully optimized by orthogonal test, and the curing process parameters of temperature and time have also been optimized. The results indicate that the optimized hydrolysis parameters for mixed silanes agent solution are as follows: V-ethanol/V-water 3 : 1, V gamma-GPS/V-BTSE 2 : 3, V-silanes 6 vol.%, pH 4.0 and hydrolysis time 72 h. In addition, the optimized curing condition for composite gamma-GPS/BTSE silane film is 120 degrees C and 30 min. After immersion in the optimized mixed gamma-GPS/BTSE silanes agent solution and curing under the optimized condition, the prepared composite gamma-GPS/BTSE silane film on Q235 steel surface can have an adhesion strength of 24.52 MPa to underlying steel substrate.
WOS研究方向Materials Science
语种英语
出版者WILEY-V C H VERLAG GMBH
WOS记录号WOS:000525608800008
内容类型期刊论文
源URL[http://ir.imr.ac.cn/handle/321006/138355]  
专题金属研究所_中国科学院金属研究所
通讯作者Sun, Z. D.
作者单位1.Chinese Acad Sci, Inst Met Res, Lab Corros & Protect Met, Shenyang 110016, Peoples R China
2.Northeastern Univ, Sch Met, Shenyang 110819, Peoples R China
3.Shenyang Inst Engn, Shenyang 110136, Peoples R China
4.Shanghai Univ, Sch Mat Sci & Engn, State Key Lab Adv Special Steel, Shanghai 200072, Peoples R China
推荐引用方式
GB/T 7714
Sun, Z. D.,Yang, Y. N.,Li, Q. K.,et al. Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235)[J]. MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK,2020,51(4):480-487.
APA Sun, Z. D.,Yang, Y. N.,Li, Q. K.,Liu, J. G.,Xu, Q.,&Yan, C. W..(2020).Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235).MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK,51(4),480-487.
MLA Sun, Z. D.,et al."Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235)".MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK 51.4(2020):480-487.
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