Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction | |
Yin, Cailiu; Huang, Qizhong; Liu, Baorong; Wang, Xiufei; Xie, Yonggui; He, Lianlong; Zhang, Mingyu; Yang, Xin | |
刊名 | MATERIALS LETTERS
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2007-08-01 | |
卷号 | 61期号:19-20页码:4015-4018 |
关键词 | hollow carbon spheres solvent-thermal reaction electron microscopy microstructure |
ISSN号 | 0167-577X |
DOI | 10.1016/j.matlet.2007.01.008 |
通讯作者 | Huang, Qizhong(qzhuang@mail.csu.edu.cn) |
英文摘要 | Fluffy hollow carbon spheres with the diameter of 0.3-1.8 mu m and shell thickness of 30-80 nm were successfully synthesized via FeCl3 catalyzed solvent-thermal reaction in a scaled autoclave at 350 degrees C for 3 h, with CaC2 and CCl4 as carbon sources and reactants. XRD and TEM observations verify that the fluffy hollow carbon spheres are composed of curved and disordered carbon flakes with the interlayer instance of approximate 0.35 nm. Furthermore, MCNTs with Fe-Mn-Cr nanorods encapsulated are also observed. A possible growth mechanism for the fluffy hollow carbon sphere is proposed. (c) 2007 Elsevier B.V. All rights reserved. |
WOS研究方向 | Materials Science ; Physics |
语种 | 英语 |
出版者 | ELSEVIER SCIENCE BV |
WOS记录号 | WOS:000248155900001 |
内容类型 | 期刊论文 |
源URL | [http://ir.imr.ac.cn/handle/321006/91196] ![]() |
专题 | 金属研究所_中国科学院金属研究所 |
通讯作者 | Huang, Qizhong |
作者单位 | 1.Guangxi Univ, Coll Phys Sci & Engn, Nanning 530004, Peoples R China 2.Cent S Univ, State Key Lab Powder Met, Changsha 410083, Peoples R China 3.Chinese Acad Sci, Inst Met Res, Shenyang Natl Lab Mat Sci, Shenyang 110016, Peoples R China |
推荐引用方式 GB/T 7714 | Yin, Cailiu,Huang, Qizhong,Liu, Baorong,et al. Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction[J]. MATERIALS LETTERS,2007,61(19-20):4015-4018. |
APA | Yin, Cailiu.,Huang, Qizhong.,Liu, Baorong.,Wang, Xiufei.,Xie, Yonggui.,...&Yang, Xin.(2007).Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction.MATERIALS LETTERS,61(19-20),4015-4018. |
MLA | Yin, Cailiu,et al."Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction".MATERIALS LETTERS 61.19-20(2007):4015-4018. |
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