Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction

doi:10.1016/j.matlet.2007.01.008

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	Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction
	Yin, Cailiu ; Huang, Qizhong ; Liu, Baorong ; Wang, Xiufei ; Xie, Yonggui ; He, Lianlong ; Zhang, Mingyu ; Yang, Xin
刊名	MATERIALS LETTERS
	2007-08-01
卷号	61 期号:19-20 页码:4015-4018
关键词	hollow carbon spheres solvent-thermal reaction electron microscopy microstructure
ISSN号	0167-577X
DOI	10.1016/j.matlet.2007.01.008
通讯作者	Huang, Qizhong(qzhuang@mail.csu.edu.cn)
英文摘要	Fluffy hollow carbon spheres with the diameter of 0.3-1.8 mu m and shell thickness of 30-80 nm were successfully synthesized via FeCl3 catalyzed solvent-thermal reaction in a scaled autoclave at 350 degrees C for 3 h, with CaC2 and CCl4 as carbon sources and reactants. XRD and TEM observations verify that the fluffy hollow carbon spheres are composed of curved and disordered carbon flakes with the interlayer instance of approximate 0.35 nm. Furthermore, MCNTs with Fe-Mn-Cr nanorods encapsulated are also observed. A possible growth mechanism for the fluffy hollow carbon sphere is proposed. (c) 2007 Elsevier B.V. All rights reserved.
WOS研究方向	Materials Science ; Physics
语种	英语
出版者	ELSEVIER SCIENCE BV
WOS记录号	WOS:000248155900001
内容类型	期刊论文
源URL	[http://ir.imr.ac.cn/handle/321006/91196]
专题	金属研究所_中国科学院金属研究所
通讯作者	Huang, Qizhong
作者单位	1.Guangxi Univ, Coll Phys Sci & Engn, Nanning 530004, Peoples R China 2.Cent S Univ, State Key Lab Powder Met, Changsha 410083, Peoples R China 3.Chinese Acad Sci, Inst Met Res, Shenyang Natl Lab Mat Sci, Shenyang 110016, Peoples R China
推荐引用方式 GB/T 7714	Yin, Cailiu,Huang, Qizhong,Liu, Baorong,et al. Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction[J]. MATERIALS LETTERS,2007,61(19-20):4015-4018.
APA	Yin, Cailiu.,Huang, Qizhong.,Liu, Baorong.,Wang, Xiufei.,Xie, Yonggui.,...&Yang, Xin.(2007).Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction.MATERIALS LETTERS,61(19-20),4015-4018.
MLA	Yin, Cailiu,et al."Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction".MATERIALS LETTERS 61.19-20(2007):4015-4018.