Efficient Determination of the Enantiomeric Purity and Absolute Configuration of Flavanones by Using (S)-3,3 '-Dibromo-1,1 '-bi-2-naphthol as a Chiral Solvating Agent

doi:10.1021/acs.jnatprod.5b00690

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	Efficient Determination of the Enantiomeric Purity and Absolute Configuration of Flavanones by Using (S)-3,3 '-Dibromo-1,1 '-bi-2-naphthol as a Chiral Solvating Agent
	Du, Guoxin 2,3; Li, Yisu 1,3; Ma, Shunan 2; Wang, Rui 2; Li, Bo 3; Guo, Fujiang 2; Zhu, Weiliang3 ; Li, Yiming 2
刊名	JOURNAL OF NATURAL PRODUCTS
	2015-12
卷号	78 期号:12 页码:2968-2974
ISSN号	0163-3864
DOI	10.1021/acs.jnatprod.5b00690
文献子类	Article
英文摘要	The enantiomeric purity and absolute configuration of flavanones were first determined using (S)-3,3'-dibromo-1,1'-bi-2-naphthol as a chiral solvating agent by means of H-1 NMR spectroscopy. The enantiomeric purity results closely matched those based on chiral HPLC analysis.
资助项目	National Natural Science Foundation of China[81173518] ; Eastern Scholar Tracking Program of Shanghai Municipal Education Commission[2012-90] ; National High Technology Research and Development Program of China (863 program)[2013AA093003] ; International Collaboration Project[2014DFA31130] ; Program of Shanghai E-institute of Bioactive Constituents in Traditional Chinese Medicine[00000000]
WOS关键词	NMR-SPECTROSCOPY ; CIRCULAR-DICHROISM ; CARBOXYLIC-ACIDS ; PRIMARY AMINES ; SHIFT-REAGENT ; HYDROXY-ACIDS ; ASSIGNMENT ; ENANTIODIFFERENTIATION ; DISCRIMINATION ; (S)-BINOL
WOS研究方向	Plant Sciences ; Pharmacology & Pharmacy
语种	英语
出版者	AMER CHEMICAL SOC
WOS记录号	WOS:000367562600013
内容类型	期刊论文
源URL	[http://119.78.100.183/handle/2S10ELR8/276297]
专题	药物发现与设计中心天然药物化学研究室
通讯作者	Li, Bo
作者单位	1.Univ Sci & Technol China, Nano Sci & Technol Inst, Suzhou 215123, Peoples R China 2.Shanghai Univ Tradit Chinese Med, Sch Pharm, Shanghai 201203, Peoples R China; 3.Chinese Acad Sci, Shanghai Inst Mat Med, CAS Key Lab Receptor Res, Shanghai 201203, Peoples R China;
推荐引用方式 GB/T 7714	Du, Guoxin,Li, Yisu,Ma, Shunan,et al. Efficient Determination of the Enantiomeric Purity and Absolute Configuration of Flavanones by Using (S)-3,3 '-Dibromo-1,1 '-bi-2-naphthol as a Chiral Solvating Agent[J]. JOURNAL OF NATURAL PRODUCTS,2015,78(12):2968-2974.
APA	Du, Guoxin.,Li, Yisu.,Ma, Shunan.,Wang, Rui.,Li, Bo.,...&Li, Yiming.(2015).Efficient Determination of the Enantiomeric Purity and Absolute Configuration of Flavanones by Using (S)-3,3 '-Dibromo-1,1 '-bi-2-naphthol as a Chiral Solvating Agent.JOURNAL OF NATURAL PRODUCTS,78(12),2968-2974.
MLA	Du, Guoxin,et al."Efficient Determination of the Enantiomeric Purity and Absolute Configuration of Flavanones by Using (S)-3,3 '-Dibromo-1,1 '-bi-2-naphthol as a Chiral Solvating Agent".JOURNAL OF NATURAL PRODUCTS 78.12(2015):2968-2974.