5-[(3,4-Dimethoxybenzyl)aminomethylene]-2,2-dimethyl-1,3-dioxane-4,6-dione

doi:10.1107/S1600536809017413

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	5-[(3,4-Dimethoxybenzyl)aminomethylene]-2,2-dimethyl-1,3-dioxane-4,6-dione
	Li, Rui 2; Shi, Jian-You 1; Ding, Zhen-Yu 2; Wei, Yu-Quan 2; Ding, Jian3
刊名	ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE
	2009-06
卷号	65 页码:O1298-U2033
ISSN号	1600-5368
DOI	10.1107/S1600536809017413
文献子类	Article
英文摘要	The title compound, C(15)H(17)NO(6), is approximately planar, with dihedral angles of 3.11 (4) and 2.12 (4)degrees between the connecting aminomethylene unit and the planar part of the dioxane ring, and between the dimethoxybenzyl ring and the aminomethylene group, respectively. The dioxane ring exhibits a half-boat conformation, in which the C atom between the dioxane O atoms is 0.5471 (8) angstrom out of the plane. The molecule has an intramolecular N-H center dot center dot center dot O hydrogen bond which may stabilize the planar conformation. In the crystal, weak intermolecular C-H center dot center dot center dot O hydrogen-bonding contacts, result in the formation of sheets parallel to the ab plane.
资助项目	State Key Laboratory of Drug Research (Shanghai Institute of Materia Medica, Chinese Academy of Sciences)[00000000]
WOS关键词	ACID
WOS研究方向	Crystallography
语种	英语
出版者	WILEY-BLACKWELL
WOS记录号	WOS:000266514400182
内容类型	期刊论文
源URL	[http://119.78.100.183/handle/2S10ELR8/279214]
专题	药理学第一研究室中科院受体结构与功能重点实验室新药研究国家重点实验室
通讯作者	Li, Rui
作者单位	1.Sichuan Univ, Dept Med Chem, W China Sch Pharm, Chengdu 610041, Peoples R China; 2.Sichuan Univ, State Key Lab Biotherapy, W China Hosp, Chengdu 610041, Peoples R China; 3.Chinese Acad Sci, State Key Lab Drug Res, Shanghai Inst Mat Med, Shanghai 201203, Peoples R China
推荐引用方式 GB/T 7714	Li, Rui,Shi, Jian-You,Ding, Zhen-Yu,et al. 5-[(3,4-Dimethoxybenzyl)aminomethylene]-2,2-dimethyl-1,3-dioxane-4,6-dione[J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE,2009,65:O1298-U2033.
APA	Li, Rui,Shi, Jian-You,Ding, Zhen-Yu,Wei, Yu-Quan,&Ding, Jian.(2009).5-[(3,4-Dimethoxybenzyl)aminomethylene]-2,2-dimethyl-1,3-dioxane-4,6-dione.ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE,65,O1298-U2033.
MLA	Li, Rui,et al."5-[(3,4-Dimethoxybenzyl)aminomethylene]-2,2-dimethyl-1,3-dioxane-4,6-dione".ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE 65(2009):O1298-U2033.