Capillary Electrophoresis Coupled with Electrochemiluminescence for the Facile Separation and Determination of Salbutamol and Clenbuterol in Urine

	Capillary Electrophoresis Coupled with Electrochemiluminescence for the Facile Separation and Determination of Salbutamol and Clenbuterol in Urine
	Bao Y ; Yang F ; Yang XR
刊名	electroanalysis
	2012
卷号	24 期号:7 页码:1597-1603
关键词	PERFORMANCE LIQUID-CHROMATOGRAPHY IONIC LIQUIDS ELECTROGENERATED CHEMILUMINESCENCE ELECTROCHEMICAL DETECTION CE-ELECTROCHEMILUMINESCENCE SOLID-PHASE CYCLODEXTRIN EXTRACTION ALKALOIDS MEDICINE
ISSN号	1040-0397
通讯作者	yang xr
中文摘要	a capillary electrophoresis coupled with tris(2,2'-bipyridyl) ruthenium(ii) (ru(bpy)32+) electrochemiluminescence detection system was developed to determine salbutamol and clenbuterol in urine. some factors that affected the performances of separation and detection were investigated. under the optimized conditions, one single quantitative analysis of salbutamol and clenbuterol was achieved at a separation voltage of 15 kv within 9 min, and the lods (s/n=3) and loqs (s/n=10) of salbutamol and clenbuterol were 8.43x10-8 mol/l, 2.61x10-7 mol/l and 2.73x10-7 mol/l, 8.21x10-7 mol/l, respectively. the recovery obtained from the analysis of spiked urine samples was between 88.6?% and 104.7?% with rsds lower than 6.70?%. the method was successfully applied to determine salbutamol and clenbuterol in urine samples.
收录类别	SCI收录期刊论文
语种	英语
WOS记录号	WOS:000305999200015
公开日期	2013-05-20
内容类型	期刊论文
源URL	[http://ir.ciac.jl.cn/handle/322003/48071]
专题	长春应用化学研究所_长春应用化学研究所知识产出_期刊论文
推荐引用方式 GB/T 7714	Bao Y,Yang F,Yang XR. Capillary Electrophoresis Coupled with Electrochemiluminescence for the Facile Separation and Determination of Salbutamol and Clenbuterol in Urine[J]. electroanalysis,2012,24(7):1597-1603.
APA	Bao Y,Yang F,&Yang XR.(2012).Capillary Electrophoresis Coupled with Electrochemiluminescence for the Facile Separation and Determination of Salbutamol and Clenbuterol in Urine.electroanalysis,24(7),1597-1603.
MLA	Bao Y,et al."Capillary Electrophoresis Coupled with Electrochemiluminescence for the Facile Separation and Determination of Salbutamol and Clenbuterol in Urine".electroanalysis 24.7(2012):1597-1603.