Enantioseparation of 2-aryl-1,3-dicarbonyl analogues by high performance liquid chromatography using polysaccharide type chiral stationary phase | |
Xu Z(许哲) ; Ding ZD(丁左定) ; Xu X(许旭) ; Xie XA(谢小安) | |
刊名 | Chirality |
2008 | |
卷号 | 20期号:2页码:147-150 |
ISSN号 | 0899-0042 |
其他题名 | Enantioseparation of 2-aryl-1,3-dicarbonyl analogues by high performance liquid chromatography using polysaccharide type chiral stationary phase |
通讯作者 | 许旭 |
英文摘要 | The HPLC chiral separation of 21 kinds of 2-aryl-1,3-dicarbonyl analogues was investigated in normal phase mode with amylose tris(3,5-dimethylphenylcarbamate), amylose tris((S)-1-phenylethylcarbamate), cellulose tris(3,5-dimethylphenylcarbamate), and cellulose tris(4-methylbenzoate) chiral stationary phases, respectively. The whole set of 2-aryl-1,3-dicarbonyl analogues shows better enantioselectivity and enantioseparation on amylose tris(3,5-dimethylphenyl carbamate) (Chiralpak AD-H). The temperature dependence of enantioselectivity was studied to improve the enantioseparation. In addition, efforts are made to relate analyte structure with the quality of the achieved chiral separation. |
学科主题 | 分析化学 |
收录类别 | SCI |
原文出处 | http://dx.doi.org/10.1002/chir.20513 |
语种 | 英语 |
WOS记录号 | WOS:000252531400013 |
公开日期 | 2013-03-12 |
内容类型 | 期刊论文 |
源URL | [http://202.127.28.38/handle/331003/24773] |
专题 | 上海有机化学研究所_上海有机化学研究所 |
推荐引用方式 GB/T 7714 | Xu Z,Ding ZD,Xu X,et al. Enantioseparation of 2-aryl-1,3-dicarbonyl analogues by high performance liquid chromatography using polysaccharide type chiral stationary phase[J]. Chirality,2008,20(2):147-150. |
APA | 许哲,丁左定,许旭,&谢小安.(2008).Enantioseparation of 2-aryl-1,3-dicarbonyl analogues by high performance liquid chromatography using polysaccharide type chiral stationary phase.Chirality,20(2),147-150. |
MLA | 许哲,et al."Enantioseparation of 2-aryl-1,3-dicarbonyl analogues by high performance liquid chromatography using polysaccharide type chiral stationary phase".Chirality 20.2(2008):147-150. |
个性服务 |
查看访问统计 |
相关权益政策 |
暂无数据 |
收藏/分享 |
除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。
修改评论