Enantioseparation of 2-aryl-1,3-dicarbonyl analogues by high performance liquid chromatography using polysaccharide type chiral stationary phase
Xu Z(许哲) ; Ding ZD(丁左定) ; Xu X(许旭) ; Xie XA(谢小安)
刊名Chirality
2008
卷号20期号:2页码:147-150
ISSN号0899-0042
其他题名Enantioseparation of 2-aryl-1,3-dicarbonyl analogues by high performance liquid chromatography using polysaccharide type chiral stationary phase
通讯作者许旭
英文摘要The HPLC chiral separation of 21 kinds of 2-aryl-1,3-dicarbonyl analogues was investigated in normal phase mode with amylose tris(3,5-dimethylphenylcarbamate), amylose tris((S)-1-phenylethylcarbamate), cellulose tris(3,5-dimethylphenylcarbamate), and cellulose tris(4-methylbenzoate) chiral stationary phases, respectively. The whole set of 2-aryl-1,3-dicarbonyl analogues shows better enantioselectivity and enantioseparation on amylose tris(3,5-dimethylphenyl carbamate) (Chiralpak AD-H). The temperature dependence of enantioselectivity was studied to improve the enantioseparation. In addition, efforts are made to relate analyte structure with the quality of the achieved chiral separation.
学科主题分析化学
收录类别SCI
原文出处http://dx.doi.org/10.1002/chir.20513
语种英语
WOS记录号WOS:000252531400013
公开日期2013-03-12
内容类型期刊论文
源URL[http://202.127.28.38/handle/331003/24773]  
专题上海有机化学研究所_上海有机化学研究所
推荐引用方式
GB/T 7714
Xu Z,Ding ZD,Xu X,et al. Enantioseparation of 2-aryl-1,3-dicarbonyl analogues by high performance liquid chromatography using polysaccharide type chiral stationary phase[J]. Chirality,2008,20(2):147-150.
APA 许哲,丁左定,许旭,&谢小安.(2008).Enantioseparation of 2-aryl-1,3-dicarbonyl analogues by high performance liquid chromatography using polysaccharide type chiral stationary phase.Chirality,20(2),147-150.
MLA 许哲,et al."Enantioseparation of 2-aryl-1,3-dicarbonyl analogues by high performance liquid chromatography using polysaccharide type chiral stationary phase".Chirality 20.2(2008):147-150.
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