Synthesis of carbon nitride powder by selective etching of TiC0.3N0.7 in chlorine-containing atmosphere at moderate temperature | |
Lv JJ(吕晋军)![]() ![]() | |
刊名 | Materials Chemistry and Physics
![]() |
2010 | |
卷号 | 123页码:264-268 |
关键词 | Nitride Etching Fourier transform infrared spectroscopy (FTIR) X-ray photo-emission spectroscopy (XPS) |
ISSN号 | 0254-0584 |
通讯作者 | 吕晋军 |
中文摘要 | We reported the synthesis of carbon nitride powder by extracting titanium from single inorganic pre-cursor TiC0.3N0.7 in chlorine-containing atmosphere at ambient pressure and temperature not exceeding500 ◦C. The TiC0.3N0.7 crystalline structure acted as a template, supplying active carbon and nitrogenatoms for carbon nitride when it was destroyed in chlorination. X-ray diffraction data showed that theobtained carbon nitride powders were amorphous, which was in good agreement with transmissionelectron microscope analysis. The composition and structure of carbon nitride powders were analyzedby employing Fourier transform infrared spectroscopy, Raman spectroscopy, and X-ray photoelectronspectroscopy. Results indicated that disorder structure was most likely for the carbon nitride powdersand the N content depended greatly on the chlorination temperature. Thermal analysis in flowing N2indicated that the mass loss started from 300 ◦C and the complete decomposition occurred at around650 ◦C, confirming the low thermal stability of the carbon nitride material. |
学科主题 | 材料科学与物理化学 |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000279305800044 |
公开日期 | 2012-09-28 |
内容类型 | 期刊论文 |
源URL | [http://210.77.64.217/handle/362003/1038] ![]() |
专题 | 兰州化学物理研究所_固体润滑国家重点实验室 |
通讯作者 | Lv JJ(吕晋军); Lv JJ(吕晋军) |
推荐引用方式 GB/T 7714 | Lv JJ,Lv JJ. Synthesis of carbon nitride powder by selective etching of TiC0.3N0.7 in chlorine-containing atmosphere at moderate temperature[J]. Materials Chemistry and Physics,2010,123:264-268. |
APA | 吕晋军,&吕晋军.(2010).Synthesis of carbon nitride powder by selective etching of TiC0.3N0.7 in chlorine-containing atmosphere at moderate temperature.Materials Chemistry and Physics,123,264-268. |
MLA | 吕晋军,et al."Synthesis of carbon nitride powder by selective etching of TiC0.3N0.7 in chlorine-containing atmosphere at moderate temperature".Materials Chemistry and Physics 123(2010):264-268. |
个性服务 |
查看访问统计 |
相关权益政策 |
暂无数据 |
收藏/分享 |
除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。
修改评论