Detection of Galanthamine in Bulbus lycoridis radiatae by Capillary Electrophoresis with an End-column Electrochemiluminescence of Tris(2,2 '-bipyridyl)ruthenium(II)

	Detection of Galanthamine in Bulbus lycoridis radiatae by Capillary Electrophoresis with an End-column Electrochemiluminescence of Tris(2,2 '-bipyridyl)ruthenium(II)
	Xiang Q ; Wang H ; Xu Y ; Sun L ; Gao Y
刊名	asian journal of chemistry
	2011
卷号	23 期号:4 页码:1553-1556
关键词	ZONE-ELECTROPHORESIS MASS SPECTROMETRY FLOS-DATURAE LIQUID GALANTAMINE ALKALOIDS PLASMA CHROMATOGRAPHY PRODUCTS UV
ISSN号	0970-7077
通讯作者	gao y
中文摘要	a capillary electrophoresis with an end-column electrochemiluminescence detection method is described for the determination of galanthamine in bulbus lycoridis radiatae without derivatization. to minimize the matrix effect and get rid of the interfering substances in crude extract of the herb, the effect of running buffer on separation and detection of galanthamine in real sample was investigated. under the optimized conditions: electrochemiluminescence detection at 1.2 v. 15 mmol/l phosphate buffer at ph 8.49, 13 kv separation voltage, the calibration of galanthamine was linear (r = 0.998) with detection limit of 1.0 x 10(-9) mol/l.
收录类别	SCI收录期刊论文
语种	英语
WOS记录号	WOS:000288465100030
公开日期	2012-06-11
内容类型	期刊论文
源URL	[http://ir.ciac.jl.cn/handle/322003/44738]
专题	长春应用化学研究所_长春应用化学研究所知识产出_期刊论文
推荐引用方式 GB/T 7714	Xiang Q,Wang H,Xu Y,et al. Detection of Galanthamine in Bulbus lycoridis radiatae by Capillary Electrophoresis with an End-column Electrochemiluminescence of Tris(2,2 '-bipyridyl)ruthenium(II)[J]. asian journal of chemistry,2011,23(4):1553-1556.
APA	Xiang Q,Wang H,Xu Y,Sun L,&Gao Y.(2011).Detection of Galanthamine in Bulbus lycoridis radiatae by Capillary Electrophoresis with an End-column Electrochemiluminescence of Tris(2,2 '-bipyridyl)ruthenium(II).asian journal of chemistry,23(4),1553-1556.
MLA	Xiang Q,et al."Detection of Galanthamine in Bulbus lycoridis radiatae by Capillary Electrophoresis with an End-column Electrochemiluminescence of Tris(2,2 '-bipyridyl)ruthenium(II)".asian journal of chemistry 23.4(2011):1553-1556.