Synthesis of Ti(3)SiC(2) by high energy ball milling and reactive sintering from Ti, Si, and C elements

CORC > 金属研究所 > 中国科学院金属研究所

	Synthesis of Ti(3)SiC(2) by high energy ball milling and reactive sintering from Ti, Si, and C elements
	F. L. Meng ; L. Chaffron ; Y. C. Zhou
刊名	Journal of Nuclear Materials
	2009
卷号	386-88 页码:647-649
关键词	powder synthesis carbide fabrication mixtures ceramics phases
ISSN号	0022-3115
中文摘要	We present an original method of preparation of nanostructured Ti(3)SiC(2) compound based on high energy ball milling and reactive sintering techniques. Starting materials are Ti, Si, and C elements. X-ray diffraction and secondary electron microscopy are used to identify the formed phases and to analyze the obtained microstructures. Lower milling intensity and shorter milling time are found as the best milling conditions in order to get an intimate mixture of the three elements without formation of detectable secondary phases. The optimized sintering temperature is equal to 1350 degrees C. A method used for minimizing the oxygen content in the final compound is presented. (c) 2008 Elsevier B.V. All rights reserved.
原文出处	://WOS:000266386900161
公开日期	2012-04-13
内容类型	期刊论文
源URL	[http://210.72.142.130/handle/321006/32203]
专题	金属研究所_中国科学院金属研究所
推荐引用方式 GB/T 7714	F. L. Meng,L. Chaffron,Y. C. Zhou. Synthesis of Ti(3)SiC(2) by high energy ball milling and reactive sintering from Ti, Si, and C elements[J]. Journal of Nuclear Materials,2009,386-88:647-649.
APA	F. L. Meng,L. Chaffron,&Y. C. Zhou.(2009).Synthesis of Ti(3)SiC(2) by high energy ball milling and reactive sintering from Ti, Si, and C elements.Journal of Nuclear Materials,386-88,647-649.
MLA	F. L. Meng,et al."Synthesis of Ti(3)SiC(2) by high energy ball milling and reactive sintering from Ti, Si, and C elements".Journal of Nuclear Materials 386-88(2009):647-649.