Synthesis of Ti(3)SiC(2) by high energy ball milling and reactive sintering from Ti, Si, and C elements | |
F. L. Meng ; L. Chaffron ; Y. C. Zhou | |
刊名 | Journal of Nuclear Materials
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2009 | |
卷号 | 386-88页码:647-649 |
关键词 | powder synthesis carbide fabrication mixtures ceramics phases |
ISSN号 | 0022-3115 |
中文摘要 | We present an original method of preparation of nanostructured Ti(3)SiC(2) compound based on high energy ball milling and reactive sintering techniques. Starting materials are Ti, Si, and C elements. X-ray diffraction and secondary electron microscopy are used to identify the formed phases and to analyze the obtained microstructures. Lower milling intensity and shorter milling time are found as the best milling conditions in order to get an intimate mixture of the three elements without formation of detectable secondary phases. The optimized sintering temperature is equal to 1350 degrees C. A method used for minimizing the oxygen content in the final compound is presented. (c) 2008 Elsevier B.V. All rights reserved. |
原文出处 | |
公开日期 | 2012-04-13 |
内容类型 | 期刊论文 |
源URL | [http://210.72.142.130/handle/321006/32203] ![]() |
专题 | 金属研究所_中国科学院金属研究所 |
推荐引用方式 GB/T 7714 | F. L. Meng,L. Chaffron,Y. C. Zhou. Synthesis of Ti(3)SiC(2) by high energy ball milling and reactive sintering from Ti, Si, and C elements[J]. Journal of Nuclear Materials,2009,386-88:647-649. |
APA | F. L. Meng,L. Chaffron,&Y. C. Zhou.(2009).Synthesis of Ti(3)SiC(2) by high energy ball milling and reactive sintering from Ti, Si, and C elements.Journal of Nuclear Materials,386-88,647-649. |
MLA | F. L. Meng,et al."Synthesis of Ti(3)SiC(2) by high energy ball milling and reactive sintering from Ti, Si, and C elements".Journal of Nuclear Materials 386-88(2009):647-649. |
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