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Crystallization and Hardness of Melt Spun Fe(73)Si(13)B(9)Nb(4)Cu(1) Alloy
J. I. Akhter ; M. Iqbal ; M. Siddique ; M. Ahmad ; M. A. Haq ; M. A. Shaikh ; Z. Q. Hu
刊名Journal of Materials Science & Technology
2009
卷号25期号:1页码:48-52
关键词Amorphous alloy Crystallization Mossbauer spectroscopy Hardness ultrafine grain-structure x-ray-diffraction magnetic-properties mossbauer-spectroscopy amorphous fe73.5cu1nb3si13.5b9 metallic glasses behavior additions niobium
ISSN号1005-0302
中文摘要An alloy having composition Fe(73)Si(13)B(9)Nb(4)Cu(1) was synthesized by melt spinning to investigate the kinetics of crystallization. Techniques of differential scanning calorimetry (DSC), X-ray diffraction (XRD) and Mossbauer spectroscopy were employed to characterize the phases produced due, to annealing at various temperatures. High temperature DSC revealed two stage crystallization reactions. First stage, crystallization occurs at temperature around 514 degrees C with the production of alpha-Fe (bcc) and Fe(3)Si phases. In the second stage, Fe(2)B and alpha-Fe (Si,Nb) phases were produced. Mossbauer results revealed the formation of Fe(3)Si, Fe(13)Si(3) and Fe(7)Si(1) in the first stage and Fe(3)Si, Fe(13)Si(3), Fe(2)B and alpha-Fe (Si,Nb) phases in the second stage of crystallization. An abrupt change in average internal magnetic field was observed at 500 degrees C. The maximum hardness value was found for the sample heat-treated at 500 degrees C.
原文出处://WOS:000263620900003
公开日期2012-04-13
内容类型期刊论文
源URL[http://210.72.142.130/handle/321006/31811]  
专题金属研究所_中国科学院金属研究所
推荐引用方式
GB/T 7714
J. I. Akhter,M. Iqbal,M. Siddique,et al. Crystallization and Hardness of Melt Spun Fe(73)Si(13)B(9)Nb(4)Cu(1) Alloy[J]. Journal of Materials Science & Technology,2009,25(1):48-52.
APA J. I. Akhter.,M. Iqbal.,M. Siddique.,M. Ahmad.,M. A. Haq.,...&Z. Q. Hu.(2009).Crystallization and Hardness of Melt Spun Fe(73)Si(13)B(9)Nb(4)Cu(1) Alloy.Journal of Materials Science & Technology,25(1),48-52.
MLA J. I. Akhter,et al."Crystallization and Hardness of Melt Spun Fe(73)Si(13)B(9)Nb(4)Cu(1) Alloy".Journal of Materials Science & Technology 25.1(2009):48-52.
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