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Experimental study on microscopic formation damage of low permeability reservoir caused by HPG fracturing fluid
Xu, Zhichao ; Li, Zhiping ; Wang, Cai ; Adenutsi, Caspar Daniel
刊名JOURNAL OF NATURAL GAS SCIENCE AND ENGINEERING
2016
关键词Formation damage HPG fracturing fluid N(2)adsorption Wettability SEM PORE STRUCTURE GAS-ADSORPTION SURFACE-AREA GEL-DAMAGE CLEANUP
DOI10.1016/j.jngse.2016.10.063
英文摘要Hydraulic fracturing has become an important stimulation technique for low/ultra-low permeability reservoirs. Research on formation damage caused by fracturing fluid has mainly focused on permeability, sensitivity, fracturing fluid and clay minerals. However, little attention has been devoted to the microscopic changes in pore structure and properties. In this paper, nitrogen gas-adsorption techniques were introduced to characterize the microscopic changes in pore structure. Meanwhile, contact angle testing and Scanning Electron Microscope (SEM) observations were also used to show the changes in wettability and surface morphology of cores, respectively. The results showed that the pore size distributions (PSDs) of low permeability cores were wide, with approximately 75% macropore volume. The obvious changes in PSDs of damaged samples occurred in the range of 2-5 nm and 30-80 nm. The specific surface area decreased, and the adsorbability of damaged samples declined, as well. Concentrated gel and solid residues were confirmed to be the main damage mechanisms for gel breaking liquids, which resulted in changes in composition and.roughness, making the cores more hydrophilic. Based on the results of the analysis, the N-2 adsorption technique is deemed appropriate for the study of reservoir formation damage when a certain amount of mesopores are present. Additionally, a new method of determining contact angles for porous media is also recommended. (C) 2016 Elsevier B.V. All rights reserved.; Beijing Municipal Natural Science Foundation [3162026]; SCI(E); ARTICLE; wendaocao123@163.com; 486-495; 36
语种英语
内容类型期刊论文
源URL[http://ir.pku.edu.cn/handle/20.500.11897/458510]  
专题工学院
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GB/T 7714
Xu, Zhichao,Li, Zhiping,Wang, Cai,et al. Experimental study on microscopic formation damage of low permeability reservoir caused by HPG fracturing fluid[J]. JOURNAL OF NATURAL GAS SCIENCE AND ENGINEERING,2016.
APA Xu, Zhichao,Li, Zhiping,Wang, Cai,&Adenutsi, Caspar Daniel.(2016).Experimental study on microscopic formation damage of low permeability reservoir caused by HPG fracturing fluid.JOURNAL OF NATURAL GAS SCIENCE AND ENGINEERING.
MLA Xu, Zhichao,et al."Experimental study on microscopic formation damage of low permeability reservoir caused by HPG fracturing fluid".JOURNAL OF NATURAL GAS SCIENCE AND ENGINEERING (2016).
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