Synthesis and crystal structure of N-(1 &apos;-Phenyl-2   &apos;-hydroxyethyl)-2,3-naphthylenedicarboximide

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	Synthesis and crystal structure of N-(1 '-Phenyl-2 '-hydroxyethyl)-2,3-naphthylenedicarboximide
	Wang, ZY ; Du, DM ; Wu, D ; Hua, WT ; Jin, XL
刊名	高等学校化学学报
	2003
关键词	naphthylene synthesis amino alcohol crystal structure COMPLEXES KETONES ACIDS
英文摘要	N-(1'-Phenyl-2'-hydroxyethyl)-2.3-naphthylenedicarboximide(1a) was obtained by the reaction of 2,3-naphthylenedicarbonitrile with R-phenylglycinol. 2, 3-Naphthylenedicarboxylic acid, when reacts with thionyl chloride, gives 2, 3-naphthalenedicarboxylic acid cyclic anhydride rather than the corresponding 2, 3-naphthalenedicarboxylic Acid dichloride. The former, when reacts with S-leucinol. gives corresponding dicarboximide(1b). The crystal structure of compound la was determined by an X-ray single crystal diffraction analysis. Compound 1a: C40H30N2()(6), F-w = 634.66, orthorhombic. space group P2(1)2(1)2(1), a = 1.15556 (5) nm, b = 3.16552 (12) nm, c = 0.85984 (3) nm; alpha = 90degrees beta = 90degrees, = 90degrees, V = 3.1452 (11) nm(3), Z = 4. F(000) 1328, D-c = 1.340 g/cm(3), mu = 0.091 mm(-1). Reflections collected/unique. 28053/4068 (R-int = 0.0411); Final R indices [I > 2sigma(I)]: R-1 = 0.0337. wR(2) = 0.0687; Largest diff. peak and hole, 248 and -222 e . nm(-3).; Chemistry, Multidisciplinary; SCI(E); EI; 中国科学引文数据库(CSCD); 0; ARTICLE; 2; 160-164; 19
语种	英语
内容类型	期刊论文
源URL	[http://ir.pku.edu.cn/handle/20.500.11897/400793]
专题	化学与分子工程学院
推荐引用方式 GB/T 7714	Wang, ZY,Du, DM,Wu, D,et al. Synthesis and crystal structure of N-(1 '-Phenyl-2 '-hydroxyethyl)-2,3-naphthylenedicarboximide[J]. 高等学校化学学报,2003.
APA	Wang, ZY,Du, DM,Wu, D,Hua, WT,&Jin, XL.(2003).Synthesis and crystal structure of N-(1 '-Phenyl-2 '-hydroxyethyl)-2,3-naphthylenedicarboximide.高等学校化学学报.
MLA	Wang, ZY,et al."Synthesis and crystal structure of N-(1 '-Phenyl-2 '-hydroxyethyl)-2,3-naphthylenedicarboximide".高等学校化学学报 (2003).