Synthesis and properties of bisnialeimide-modified novolak resin/silsesquioxane nanocomposites | |
Lu, GT; Huang, Y; Yan, YH; Zhao, T; Yu, YZ | |
刊名 | JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY
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2003-08-15 | |
卷号 | 41期号:16页码:2599-2606 |
关键词 | Nanocomposites Silsesquioxane Sol-gel Process N-gamma-triethoxylsilylpropyl-maleamic Acid Bismaleimide-modified Novolak Resins |
ISSN号 | 0887-624X |
DOI | 10.1002/pola.10786 |
英文摘要 | Bismaleimide-modified novolak resin/silsesquioxane (BMI-PN/SiO3/2) nanocomposites were prepared by the sol-gel process. The reactions in the sol-gel synthesis were characterized by Fourier transform infrared spectroscopy. It was found by field emission scanning electron microscopy and atomic force microscopy studies that the particle size of the dispersed phase was about 100 nm, and there existed particle aggregates. The proportion of bismaleimide in the BMI-PN/SiO3/2 nanocomposites showed an important effect on the thermal properties of the composites, as demonstrated by thermogravimetric analysis and dynamical mechanical analysis. Major improvements in the glass-transition temperature and the heat resistance of the material were achieved by the introduction of the nanosized SiO3/2 inorganic phase, and the modulus at high temperatures was improved too. (C) 2003 Wiley Periodicals, Inc. |
语种 | 英语 |
出版者 | JOHN WILEY & SONS INC |
WOS记录号 | WOS:000184408800017 |
内容类型 | 期刊论文 |
源URL | [http://ir.iccas.ac.cn/handle/121111/80515] ![]() |
专题 | 中国科学院化学研究所 |
通讯作者 | Lu, GT |
作者单位 | Chinese Acad Sci, Inst Chem, Ctr Mol Sci, Beijing 100080, Peoples R China |
推荐引用方式 GB/T 7714 | Lu, GT,Huang, Y,Yan, YH,et al. Synthesis and properties of bisnialeimide-modified novolak resin/silsesquioxane nanocomposites[J]. JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY,2003,41(16):2599-2606. |
APA | Lu, GT,Huang, Y,Yan, YH,Zhao, T,&Yu, YZ.(2003).Synthesis and properties of bisnialeimide-modified novolak resin/silsesquioxane nanocomposites.JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY,41(16),2599-2606. |
MLA | Lu, GT,et al."Synthesis and properties of bisnialeimide-modified novolak resin/silsesquioxane nanocomposites".JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY 41.16(2003):2599-2606. |
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