Drawing-induced Crystallization Behavior and Brill Transition of Nylon 1010 | |
Wang Ji-Ku1; Zhao Guo-Sheng1; Zhou Yun-Chun2 | |
刊名 | CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE
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2011-05-10 | |
卷号 | 32期号:5页码:1225-1230 |
关键词 | Nylon 1010 Draw-induced Crystallization Brill Transition Crystal Orientation |
ISSN号 | 0251-0790 |
英文摘要 | The crystal transitions and crystal orientations of Nylon 1010 drawing-induced at different drawing temperatures(T(d)) and drawing ratios(lambda) were studied by Differential Scanning Calorimetry(DSC), Wide-Angle X-ray Diffraction(WAXD) and two dimensional (2D) WAXD experiments. The results show that drawing is favorable to the transition of delta' form from a form of Nylon 1010 and so-called Brill transition became more obviously with drawing ratio increasing under the same temperature. New relationship of crystal form versus temperature was first discovered in which delta' form of Nylon 1010 could be gradually transformed into a form when drawn at higher drawing temperature. This is distincted from the crystallization performance of Nylon 1010 under thermal effect without drawing. The measurements of orientation degrees, based on 2D WAXS experiments, showed that crystal orientations were solely decided by the drawing ratios. Furthermore, the d spacing of (002) reflections increased with the drawing ratios, which also showed the dependence of long axis increasment on the drawing orientation. |
语种 | 英语 |
出版者 | HIGHER EDUCATION PRESS |
WOS记录号 | WOS:000291175800042 |
内容类型 | 期刊论文 |
源URL | [http://ir.iccas.ac.cn/handle/121111/72451] ![]() |
专题 | 中国科学院化学研究所 |
通讯作者 | Wang Ji-Ku |
作者单位 | 1.Jilin Normal Univ, Coll Chem, Siping 136000, Peoples R China 2.Chinese Acad Sci, Changchun Inst Appl Chem, State Key Lab Polymer Phys & Chem, Changchun 130022, Peoples R China |
推荐引用方式 GB/T 7714 | Wang Ji-Ku,Zhao Guo-Sheng,Zhou Yun-Chun. Drawing-induced Crystallization Behavior and Brill Transition of Nylon 1010[J]. CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,2011,32(5):1225-1230. |
APA | Wang Ji-Ku,Zhao Guo-Sheng,&Zhou Yun-Chun.(2011).Drawing-induced Crystallization Behavior and Brill Transition of Nylon 1010.CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,32(5),1225-1230. |
MLA | Wang Ji-Ku,et al."Drawing-induced Crystallization Behavior and Brill Transition of Nylon 1010".CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE 32.5(2011):1225-1230. |
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