ENANTIOMERIC SEPARATION OF ALPHA-PHENYLETHYLAMINE AND ITS SUBSTITUTED ISOMERS BY GAS-CHROMATOGRAPHY | |
LOU, XW; LIU, XL; ZHANG, SZ; ZHOU, LM | |
刊名 | JOURNAL OF CHROMATOGRAPHY
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1991-11-08 | |
卷号 | 586期号:1页码:139-144 |
ISSN号 | 0021-9673 |
文献子类 | Article |
英文摘要 | Alpha-phenylethylamine, o, m, p-methoxy-alpha-phenylethylamines and o, m, p-methyl-alpha-phenylethylamines were enantiomerically separated with four different diamide chiral stationary phases (CSPs) [monobenzyl succinate-L-Val-tert.-butylamide (CSP-1), undecenoyl-L-Val-S-alpha-phenylethylamide (CSP-2), undecenoyl-L-Val-R-alpha-phenylethylamide (CSP-3) and cross-linked polycyanoethyl vinyl siloxane-L-Val-tert.-butylamide (CSP-4)] using capillary gas chromatography. The ortho-effect of the methoxy group on the enantiomeric separation was investigated. The elution order of the enantiomers on CSP-3 is reversed with respect to that on the other CSPs studied. The enantiomeric separation of alpha-phenylethylamine and its methoxy- and methyl-substituted isomers is illustrated. |
WOS研究方向 | Chemistry |
语种 | 英语 |
出版者 | ELSEVIER SCIENCE BV |
WOS记录号 | WOS:A1991GR29300014 |
内容类型 | 期刊论文 |
源URL | [http://cas-ir.dicp.ac.cn/handle/321008/167638] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | CHINESE ACAD SCI,DALIAN INST CHEM PHYS,DALIAN 116012,PEOPLES R CHINA |
推荐引用方式 GB/T 7714 | LOU, XW,LIU, XL,ZHANG, SZ,et al. ENANTIOMERIC SEPARATION OF ALPHA-PHENYLETHYLAMINE AND ITS SUBSTITUTED ISOMERS BY GAS-CHROMATOGRAPHY[J]. JOURNAL OF CHROMATOGRAPHY,1991,586(1):139-144. |
APA | LOU, XW,LIU, XL,ZHANG, SZ,&ZHOU, LM.(1991).ENANTIOMERIC SEPARATION OF ALPHA-PHENYLETHYLAMINE AND ITS SUBSTITUTED ISOMERS BY GAS-CHROMATOGRAPHY.JOURNAL OF CHROMATOGRAPHY,586(1),139-144. |
MLA | LOU, XW,et al."ENANTIOMERIC SEPARATION OF ALPHA-PHENYLETHYLAMINE AND ITS SUBSTITUTED ISOMERS BY GAS-CHROMATOGRAPHY".JOURNAL OF CHROMATOGRAPHY 586.1(1991):139-144. |
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