ENANTIOMERIC SEPARATION OF ALPHA-PHENYLETHYLAMINE AND ITS SUBSTITUTED ISOMERS BY GAS-CHROMATOGRAPHY

	ENANTIOMERIC SEPARATION OF ALPHA-PHENYLETHYLAMINE AND ITS SUBSTITUTED ISOMERS BY GAS-CHROMATOGRAPHY
	LOU, XW; LIU, XL; ZHANG, SZ; ZHOU, LM
刊名	JOURNAL OF CHROMATOGRAPHY
	1991-11-08
卷号	586 期号:1 页码:139-144
ISSN号	0021-9673
文献子类	Article
英文摘要	Alpha-phenylethylamine, o, m, p-methoxy-alpha-phenylethylamines and o, m, p-methyl-alpha-phenylethylamines were enantiomerically separated with four different diamide chiral stationary phases (CSPs) [monobenzyl succinate-L-Val-tert.-butylamide (CSP-1), undecenoyl-L-Val-S-alpha-phenylethylamide (CSP-2), undecenoyl-L-Val-R-alpha-phenylethylamide (CSP-3) and cross-linked polycyanoethyl vinyl siloxane-L-Val-tert.-butylamide (CSP-4)] using capillary gas chromatography. The ortho-effect of the methoxy group on the enantiomeric separation was investigated. The elution order of the enantiomers on CSP-3 is reversed with respect to that on the other CSPs studied. The enantiomeric separation of alpha-phenylethylamine and its methoxy- and methyl-substituted isomers is illustrated.
WOS研究方向	Chemistry
语种	英语
出版者	ELSEVIER SCIENCE BV
WOS记录号	WOS:A1991GR29300014
内容类型	期刊论文
源URL	[http://cas-ir.dicp.ac.cn/handle/321008/167638]
专题	大连化学物理研究所_中国科学院大连化学物理研究所
作者单位	CHINESE ACAD SCI,DALIAN INST CHEM PHYS,DALIAN 116012,PEOPLES R CHINA
推荐引用方式 GB/T 7714	LOU, XW,LIU, XL,ZHANG, SZ,et al. ENANTIOMERIC SEPARATION OF ALPHA-PHENYLETHYLAMINE AND ITS SUBSTITUTED ISOMERS BY GAS-CHROMATOGRAPHY[J]. JOURNAL OF CHROMATOGRAPHY,1991,586(1):139-144.
APA	LOU, XW,LIU, XL,ZHANG, SZ,&ZHOU, LM.(1991).ENANTIOMERIC SEPARATION OF ALPHA-PHENYLETHYLAMINE AND ITS SUBSTITUTED ISOMERS BY GAS-CHROMATOGRAPHY.JOURNAL OF CHROMATOGRAPHY,586(1),139-144.
MLA	LOU, XW,et al."ENANTIOMERIC SEPARATION OF ALPHA-PHENYLETHYLAMINE AND ITS SUBSTITUTED ISOMERS BY GAS-CHROMATOGRAPHY".JOURNAL OF CHROMATOGRAPHY 586.1(1991):139-144.