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High-density magnetite nanoparticles located in carbon hollow microspheres with good dispersibility and durability: their one-pot preparation and magnetic properties
Zheng, Rongbo1,2; Meng, Xianwei1; Tang, Fangqiong1
刊名European journal of inorganic chemistry
2009-07-01
期号20页码:3003-3007
关键词Materials science Nanostructures Magnetic properties Hollow spheres Iron Magnetite
ISSN号1434-1948
DOI10.1002/ejic.200900078
通讯作者Tang, fangqiong(tangfq@mail.ipc.ac.cn)
英文摘要We report, for the first time, a one-step, rapid, template-free and continuous strategy for synthesising high-density magnetite (fe(3)o(4)) nanoparticles located in carbon hollow microspheres (mchms) in which fe(3)o(4) nanoparticles (8-20 nm) are randomly dispersed in the shells of carbon hollow microspheres. the synthesis is achieved through ultrasonic spray pyrolysis of aqueous solutions containing ferrous chloride and citric acid. interestingly, it was found that there are some pores (2-6 nm) in the carbon shell. magnetic hysteresis loop measurements show that the saturation magnetisation of mchms is as high as 48.2 emu g(-1) which probably makes them more pliable to manipulation by the external magnetic field. most importantly, because of the presence of carbon on their surfaces, mchms not only exhibit good resistance to acid but can also be easily dispersed in both polar and non-polar solvents. ((c) wiley-vch verlag gmbh & co. kgaa, 69451 weinheim, germany, 2009)
WOS关键词ULTRASONIC SPRAY-PYROLYSIS ; FE3O4 NANOPARTICLES ; SPHERES ; NANOSPHERES ; SHELL ; FABRICATION ; PARTICLES ; SYSTEM
WOS研究方向Chemistry
WOS类目Chemistry, Inorganic & Nuclear
语种英语
出版者WILEY-V C H VERLAG GMBH
WOS记录号WOS:000268290000014
内容类型期刊论文
URI标识http://www.corc.org.cn/handle/1471x/2397880
专题中国科学院大学
通讯作者Tang, Fangqiong
作者单位1.Chinese Acad Sci, Tech Inst Phys & Chem, Beijing 100190, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China
推荐引用方式
GB/T 7714
Zheng, Rongbo,Meng, Xianwei,Tang, Fangqiong. High-density magnetite nanoparticles located in carbon hollow microspheres with good dispersibility and durability: their one-pot preparation and magnetic properties[J]. European journal of inorganic chemistry,2009(20):3003-3007.
APA Zheng, Rongbo,Meng, Xianwei,&Tang, Fangqiong.(2009).High-density magnetite nanoparticles located in carbon hollow microspheres with good dispersibility and durability: their one-pot preparation and magnetic properties.European journal of inorganic chemistry(20),3003-3007.
MLA Zheng, Rongbo,et al."High-density magnetite nanoparticles located in carbon hollow microspheres with good dispersibility and durability: their one-pot preparation and magnetic properties".European journal of inorganic chemistry .20(2009):3003-3007.
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