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	Determination of arsenic in lead-based alloy using hydride generation-atomic fluorescence spectrometry
	Song Xue-Jie; Guo Peng-Ran; Chen Hang-Ting; Duan Tai-Cheng
刊名	Chinese journal of analytical chemistry
	2007-08-01
卷号	35期号:8页码:1183-1186
关键词	Arsenic Lead-based alloy Hydride generation Atomic fluorescence spectrometry
ISSN号	0253-3820
通讯作者	Duan tai-cheng(tcduan@ciac.jl.cn)
英文摘要	A simple method based on hydride generation ( hg) -afs for the determination of as in lead-based alloys was developed. interferences caused by co-existing elements were investigated and minimized successfully. the conditions for the hydride generation technique and instrumental parameters were also optimized. kbh4 concentration was fixed in 1.0% (m/v). optimized hcl concentration in the sample and carrier solution was 10% ( v/v) and 5% (v/v), respectively. experiments showed that no interference caused by cu was observed when thiourea existed and interferences caused by sb, sri and bi could be eliminated by absorbing their corresponding hydrides using 0.5 % (m/v) kmno4 solution on-line. feasibility of this method was demonstrated by determination of two certified lead-based alloys, and the results obtained by standard addition agreed well with certified values. the method detection limit was 0.17 mu g/l and rsd was 1.5% for i i consecutive determinations of 40 mu g/l as standard solution.
WOS关键词	PLASMA-MASS SPECTROMETRY ; ABSORPTION-SPECTROMETRY ; TELLURIUM ; SELENIUM ; INTERFERENCE ; BISMUTH ; SAMPLES ; ANTIMONY ; WATER ; TRACE
WOS研究方向	Chemistry
WOS类目	Chemistry, Analytical
语种	英语
出版者	SCIENCE CHINA PRESS
WOS记录号	WOS:000250426600021
内容类型	期刊论文
URI标识	http://www.corc.org.cn/handle/1471x/2381134
专题	中国科学院大学
通讯作者	Duan Tai-Cheng
作者单位	1.Chinese Acad Sci, Changchun Inst Appl Chem, Natl Anal Res Ctr Electrochem & Spectoscopy, State Key Lab Electroanalyt Chem, Changchun 130022, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China
推荐引用方式 GB/T 7714	Song Xue-Jie,Guo Peng-Ran,Chen Hang-Ting,et al. Determination of arsenic in lead-based alloy using hydride generation-atomic fluorescence spectrometry[J]. Chinese journal of analytical chemistry,2007,35(8):1183-1186.
APA	Song Xue-Jie,Guo Peng-Ran,Chen Hang-Ting,&Duan Tai-Cheng.(2007).Determination of arsenic in lead-based alloy using hydride generation-atomic fluorescence spectrometry.Chinese journal of analytical chemistry,35(8),1183-1186.
MLA	Song Xue-Jie,et al."Determination of arsenic in lead-based alloy using hydride generation-atomic fluorescence spectrometry".Chinese journal of analytical chemistry 35.8(2007):1183-1186.

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