Indirect determination of fe(iii) in synthetic samples and iron dextran tablets by capillary electrophoresis with ultraviolet detection | |
Tang, YJ; Wu, MJ; Xu, YH | |
刊名 | Journal of aoac international
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2006 | |
卷号 | 89期号:1页码:210-213 |
ISSN号 | 1060-3271 |
通讯作者 | Wu, mj(wumj123@hotmail.com) |
英文摘要 | A capillary electrophoresis method based on the oxidation of ascorbic acid is proposed for the indirect determination of fe(iii). fe(iii) concentration corresponds to the decrease in ascorbic acid peak area. the calibration graph was linear in the range of 1.68-112 mg/l for fe(iii), which was easily detected at a concentration of 1.12 mg/l at 3 times the standard deviation of the blank divided by the slope of the calibration graph. the lack of interferences from fe(ii) in synthetic samples and 3 excipients (starch, magnesium strearate, and microcrystalline cellulose) in dextran tablets in the determination of fe(iii) confirmed the high selectivity of the proposed method. its application to the determination of fe(iii) in several synthetic samples and iron dextran tablets produced excellent results. |
WOS关键词 | ATOMIC-ABSORPTION SPECTROMETRY ; STANDARD ADDITION METHOD ; SIMULTANEOUS KINETIC DETERMINATION ; SPECTROPHOTOMETRIC DETERMINATION ; ASCORBIC-ACID ; INJECTION-ANALYSIS ; FLOW-INJECTION ; IRON(III) ; SYSTEM |
WOS研究方向 | Chemistry ; Food Science & Technology |
WOS类目 | Chemistry, Analytical ; Food Science & Technology |
语种 | 英语 |
出版者 | AOAC INT |
WOS记录号 | WOS:000235175000033 |
内容类型 | 期刊论文 |
URI标识 | http://www.corc.org.cn/handle/1471x/2379814 |
专题 | 中国科学院大学 |
通讯作者 | Wu, MJ |
作者单位 | 1.Chinese Acad Sci, Changchun Inst Appl Chem, Natl Analyt Res Ctr Electrochem & Spect, Changchun 130022, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China |
推荐引用方式 GB/T 7714 | Tang, YJ,Wu, MJ,Xu, YH. Indirect determination of fe(iii) in synthetic samples and iron dextran tablets by capillary electrophoresis with ultraviolet detection[J]. Journal of aoac international,2006,89(1):210-213. |
APA | Tang, YJ,Wu, MJ,&Xu, YH.(2006).Indirect determination of fe(iii) in synthetic samples and iron dextran tablets by capillary electrophoresis with ultraviolet detection.Journal of aoac international,89(1),210-213. |
MLA | Tang, YJ,et al."Indirect determination of fe(iii) in synthetic samples and iron dextran tablets by capillary electrophoresis with ultraviolet detection".Journal of aoac international 89.1(2006):210-213. |
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