Synthesis and glycosyllation of pyrimidin-2-yl 1-thio-alpha-D-manno- and -alpha-L-rhamnopyranoside | |
Ding, XL; Yang, GB; Kong, FZ | |
刊名 | CARBOHYDRATE RESEARCH
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1998 | |
卷号 | 310期号:2015-01-02页码:135-139 |
关键词 | Pyrimidin-2-yl 1-thio-alpha-d-mannopyranoside 1-thio-alpha-l-rhamnopyranoside |
DOI | 10.1016/S0008-6215(98)00164-5 |
英文摘要 | Pyrimidin-2-yl 2,3,4,6-tetra-O-benzyl-1-thio-alpha-D-mannopyrano side (9), pyrimidin-2-yl 2,3,4-tri-O-benzyl-alpha-L-rhamnopyranoside (10), pyrimidin-2-yl 2-O-acetyl-3,4,6-tri-O-benzyl-1-thio-alpha-D-mannopyranoside (7), and pyrimidin-2-y1 2-O-acetyl-3,4-di-O-benzyl-1-thio-alpha-L-rhamnopyranoside (8) were prepared almost quantitatively fi om the corresponding protected 1,2-O-methoxyethylidene-beta-D-manno-or-beta-L-rhamnopyranose with 2-mercaptopyrimidine in the presence of mercuric bromide. Coupling reactions of the thioglycosides promoted by silver triflate with suitable glycosyl accepters afforded 1,2-trans linked disaccharides. (C) 1998 Published by Elsevier Science Ltd. All rights reserved. |
WOS研究方向 | Biochemistry & Molecular Biology ; Chemistry |
WOS记录号 | WOS:000076439100017 |
内容类型 | 期刊论文 |
源URL | [http://ir.rcees.ac.cn/handle/311016/24297] ![]() |
专题 | 生态环境研究中心_中国科学院环境生物技术重点实验室 |
推荐引用方式 GB/T 7714 | Ding, XL,Yang, GB,Kong, FZ. Synthesis and glycosyllation of pyrimidin-2-yl 1-thio-alpha-D-manno- and -alpha-L-rhamnopyranoside[J]. CARBOHYDRATE RESEARCH,1998,310(2015-01-02):135-139. |
APA | Ding, XL,Yang, GB,&Kong, FZ.(1998).Synthesis and glycosyllation of pyrimidin-2-yl 1-thio-alpha-D-manno- and -alpha-L-rhamnopyranoside.CARBOHYDRATE RESEARCH,310(2015-01-02),135-139. |
MLA | Ding, XL,et al."Synthesis and glycosyllation of pyrimidin-2-yl 1-thio-alpha-D-manno- and -alpha-L-rhamnopyranoside".CARBOHYDRATE RESEARCH 310.2015-01-02(1998):135-139. |
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