In Situ Measurement of the Enantiomeric Excess of Alcohols and Amines under Asymmetric Reduction Reaction by H-1 NMR | |
Ye, Xiaoxia; Lei, Xinxiang; Chen, Zhenfei; Zhang, Lixue; Zhang, Anjiang; Lei, XX, Wenzhou Univ, Coll Chem & Mat Engn, Wenzhou 325035, Peoples R China | |
刊名 | ORGANIC LETTERS |
2010 | |
卷号 | 12期号:14页码:3238-3241 |
ISSN号 | 1523-7060 |
产权排序 | 3 |
英文摘要 | H-1 NMR, in situ, determines the enantiomeric excess of reduced chiral alcohols or amines without adding any auxiliary and workup. The percent ee data determined by this method agree well with those given by HPLC. This approach may be potentially applicable to many asymmetric reductions. |
学科主题 | Chemistry, Organic |
语种 | 英语 |
WOS记录号 | WOS:000279569600033 |
资助机构 | NSFC [30900129]; ZJNSFC [Y2080331, Y406386]; ZJST [2009C34014]; WZST [H20080052] ; NSFC [30900129]; ZJNSFC [Y2080331, Y406386]; ZJST [2009C34014]; WZST [H20080052] ; NSFC [30900129]; ZJNSFC [Y2080331, Y406386]; ZJST [2009C34014]; WZST [H20080052] ; NSFC [30900129]; ZJNSFC [Y2080331, Y406386]; ZJST [2009C34014]; WZST [H20080052] |
公开日期 | 2011-07-08 |
内容类型 | 期刊论文 |
源URL | [http://210.75.237.14/handle/351003/18403] |
专题 | 成都生物研究所_天然产物研究 |
通讯作者 | Lei, XX, Wenzhou Univ, Coll Chem & Mat Engn, Wenzhou 325035, Peoples R China |
推荐引用方式 GB/T 7714 | Ye, Xiaoxia,Lei, Xinxiang,Chen, Zhenfei,et al. In Situ Measurement of the Enantiomeric Excess of Alcohols and Amines under Asymmetric Reduction Reaction by H-1 NMR[J]. ORGANIC LETTERS,2010,12(14):3238-3241. |
APA | Ye, Xiaoxia,Lei, Xinxiang,Chen, Zhenfei,Zhang, Lixue,Zhang, Anjiang,&Lei, XX, Wenzhou Univ, Coll Chem & Mat Engn, Wenzhou 325035, Peoples R China.(2010).In Situ Measurement of the Enantiomeric Excess of Alcohols and Amines under Asymmetric Reduction Reaction by H-1 NMR.ORGANIC LETTERS,12(14),3238-3241. |
MLA | Ye, Xiaoxia,et al."In Situ Measurement of the Enantiomeric Excess of Alcohols and Amines under Asymmetric Reduction Reaction by H-1 NMR".ORGANIC LETTERS 12.14(2010):3238-3241. |
个性服务 |
查看访问统计 |
相关权益政策 |
暂无数据 |
收藏/分享 |
除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。
修改评论