Poly(styrene-co-N-methacryloyl-l-phenylalanine methyl ester)-functionalized magnetic nanoparticles as sorbents for the analysis of sodium benzoate in beverages
Ji, Shilei1,2; Li, Nan2,3; Qi, Li2,3; Wang, Minglin1
刊名JOURNAL OF SEPARATION SCIENCE
2017
卷号40期号:2页码:466-471
关键词Beverages Food Preservatives High-performance Liquid Chromatography Magnetic Solid-phase Extraction Sodium Benzoate
英文摘要In this study, poly(styrene-co-N-methacryloyl-l-phenylalanine methyl ester)-functionalized magnetic nanoparticles were constructed and used as magnetic solid-phase extraction sorbents for analysis of food preservatives in beverages. To prepare the poly(amino acid)-based sorbents, N-methacryloyl-l-phenylalanine methyl ester, and styrene served as the functional monomers and modified onto the magnetic nanoparticles via free radical polymerization. Interestingly, compared with propylparaben and potassium sorbate, the proposed poly(amino acid)-based sorbents showed a good selectivity to sodium benzoate. The adsorption capacity of the sorbents to sodium benzoate was 6.08 +/- 0.31 mg/g. Moreover, the fast adsorption equilibrium could be reached within 5 min. Further, the resultant poly(amino acid)-based sorbents were applied in the analysis of sodium benzoate in real beverage samples. The results proved that the proposed magnetic solid-phase extraction sorbents have a great potential for the analysis of preservatives in food samples.
语种英语
内容类型期刊论文
源URL[http://ir.iccas.ac.cn/handle/121111/38120]  
专题化学研究所_活体分析化学实验室
作者单位1.Shandong Agr Univ, Coll Food Sci & Engn, Tai An, Shandong, Peoples R China
2.Chinese Acad Sci, Beijing Natl Lab Mol Sci, Inst Chem, Key Lab Analyt Chem Living Biosyst, Beijing 100190, Peoples R China
3.Univ Chinese Acad Sci, Beijing, Peoples R China
推荐引用方式
GB/T 7714
Ji, Shilei,Li, Nan,Qi, Li,et al. Poly(styrene-co-N-methacryloyl-l-phenylalanine methyl ester)-functionalized magnetic nanoparticles as sorbents for the analysis of sodium benzoate in beverages[J]. JOURNAL OF SEPARATION SCIENCE,2017,40(2):466-471.
APA Ji, Shilei,Li, Nan,Qi, Li,&Wang, Minglin.(2017).Poly(styrene-co-N-methacryloyl-l-phenylalanine methyl ester)-functionalized magnetic nanoparticles as sorbents for the analysis of sodium benzoate in beverages.JOURNAL OF SEPARATION SCIENCE,40(2),466-471.
MLA Ji, Shilei,et al."Poly(styrene-co-N-methacryloyl-l-phenylalanine methyl ester)-functionalized magnetic nanoparticles as sorbents for the analysis of sodium benzoate in beverages".JOURNAL OF SEPARATION SCIENCE 40.2(2017):466-471.
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