Crystal Structure and New Approach to Spiro[1,3-dioxolane-2,3 '-indolin]-2 '-one | |
Chen, Gang1; Meng, Mei1; Tang, Ying1; Hao, Xiao-jiang2![]() | |
刊名 | HETEROCYCLIC COMMUNICATIONS
![]() |
2010 | |
卷号 | 16期号:2-3页码:137-143 |
关键词 | Isatin 2-chloroethanol Intermolecular Substitution Reaction Spiro[1 3-dioxolane-2 3 '-indolin]-2 '-one |
ISSN号 | 0793-0283 |
文献子类 | Article |
英文摘要 | The title compounds, spiro[1,3-dioxolane-2,3'-indolin]-2'-one, was synthesized with isatin and 2-chloroethanol by a intramolecular substitution reaction in the presence of K(2)CO(3) for the first time, which avoided the using of H(+) as catalyst in traditional synthesis of ketal compounds. The structure of spiro[1,3-dioxolane-2,3'-indolin]-2'-one was studied by X-ray single crystal diffraction, and the two byproducts in the reaction were characterized by H(1)-NMR, MS spectrums. With these results, the proposed way to spiro[1,3-dioxolane-2,3'-indolin]-2'-one and the two byproducts was brought forward. |
学科主题 | Chemistry, Organic |
WOS关键词 | INHIBITORS |
WOS研究方向 | Chemistry |
语种 | 英语 |
WOS记录号 | WOS:000286686000009 |
资助机构 | Scientific Research Foundation for PhD of Xi'an Shiyou University [Z08008]; Shaanxi Science and Technology Department [SJ08B20]; Shaanxi Education Department [09JK702] |
公开日期 | 2012-03-21 |
内容类型 | 期刊论文 |
源URL | [http://ir.kib.ac.cn:8080/handle/151853/4952] ![]() |
专题 | 昆明植物研究所_植物化学与西部植物资源持续利用国家重点实验室 |
作者单位 | 1.Xian Shiyou Univ, Coll Chem & Chem Engn, Xian 710065, Peoples R China 2.Chinese Acad Sci, State Key Lab Phytochem & Plant Resources W China, Kunming Inst Bot, Kunming 650204, Peoples R China |
推荐引用方式 GB/T 7714 | Chen, Gang,Meng, Mei,Tang, Ying,et al. Crystal Structure and New Approach to Spiro[1,3-dioxolane-2,3 '-indolin]-2 '-one[J]. HETEROCYCLIC COMMUNICATIONS,2010,16(2-3):137-143. |
APA | Chen, Gang,Meng, Mei,Tang, Ying,&Hao, Xiao-jiang.(2010).Crystal Structure and New Approach to Spiro[1,3-dioxolane-2,3 '-indolin]-2 '-one.HETEROCYCLIC COMMUNICATIONS,16(2-3),137-143. |
MLA | Chen, Gang,et al."Crystal Structure and New Approach to Spiro[1,3-dioxolane-2,3 '-indolin]-2 '-one".HETEROCYCLIC COMMUNICATIONS 16.2-3(2010):137-143. |
个性服务 |
查看访问统计 |
相关权益政策 |
暂无数据 |
收藏/分享 |
除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。
修改评论