Combined chemical separation of Lu, Hf, Rb, Sr, Sm and Nd from a single rock digest and precise and accurate isotope determinations of Lu-Hf, Rb-Sr and Sm-Nd isotope systems using Multi-Collector ICP-MS and TIMS | |
Yang, Yue-heng1,2; Zhang, Hong-fu1; Chu, Zhu-yin1,2; Xie, Lie-wen1; Wu, Fu-yuan1 | |
刊名 | INTERNATIONAL JOURNAL OF MASS SPECTROMETRY
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2010-02-15 | |
卷号 | 290期号:2-3页码:120-126 |
关键词 | Chromatography Isotope dilution Lu-Hf Rb-Sr Sm-Nd Geological samples MC-ICP-MS TIMS |
ISSN号 | 1387-3806 |
DOI | 10.1016/j.ijms.2009.12.011 |
文献子类 | Article |
英文摘要 | A combined procedure for separating Lu, Hf, Rb, Sr, Sm and Nd from a single sample digestion is presented in this paper. The procedure consists of the following four steps: (1) sample dissolution in a mixture of concentrated HF-HNO3-HClO4; (2) Lu and Hf separation from the Rb, Sr, LMREE and other matrix elements by HF-free extraction chromatography: (3) Rb, Sr and LMREE separation from other matrix elements using a cation-exchange resin; (4) Sm and Nd separation from others LMREE by extraction chromatography. Analytical feasibility, flexibility and reproducibility of Rb-Sr. Sm-Nd and Lu-Hf isotope systems are demonstrated for international standard solutions and Certified Reference Materials (CRMs). Results show good agreement with previously reported values by isotope dilution methods, indicating the technique has fewer problems in respect to well-known sample inhomogeneity of natural geological materials and demonstrating its potential application to the study of limited and precious terrestrial rocks or minerals (like peridotite, kimberlite and xenoliths) and extra-terrestrial samples (like lunar rock and meteorites). (C) 2009 Elsevier B.V. All rights reserved. |
WOS关键词 | REFERENCE MATERIALS BCR-1 ; EXTRACTION CHROMATOGRAPHY ; MASS-SPECTROMETRY ; REFERENCE SAMPLES ; SILICATE ROCKS ; TRACE-ELEMENTS ; RATIOS ; HF-176/HF-177 ; GEOCHEMISTRY ; NEODYMIUM |
WOS研究方向 | Physics ; Spectroscopy |
语种 | 英语 |
出版者 | ELSEVIER SCIENCE BV |
WOS记录号 | WOS:000275258700008 |
资助机构 | Natural Science Foundation of China(40773008 ; Natural Science Foundation of China(40773008 ; Natural Science Foundation of China(40773008 ; Natural Science Foundation of China(40773008 ; Innovation Program of Chinese Academy of Sciences(KZCX2-YW-103) ; Innovation Program of Chinese Academy of Sciences(KZCX2-YW-103) ; Innovation Program of Chinese Academy of Sciences(KZCX2-YW-103) ; Innovation Program of Chinese Academy of Sciences(KZCX2-YW-103) ; Institute of Geology and Geophysics, Chinese Academy of Sciences(ZC0903) ; Institute of Geology and Geophysics, Chinese Academy of Sciences(ZC0903) ; Institute of Geology and Geophysics, Chinese Academy of Sciences(ZC0903) ; Institute of Geology and Geophysics, Chinese Academy of Sciences(ZC0903) ; 40873008) ; 40873008) ; 40873008) ; 40873008) ; Natural Science Foundation of China(40773008 ; Natural Science Foundation of China(40773008 ; Natural Science Foundation of China(40773008 ; Natural Science Foundation of China(40773008 ; Innovation Program of Chinese Academy of Sciences(KZCX2-YW-103) ; Innovation Program of Chinese Academy of Sciences(KZCX2-YW-103) ; Innovation Program of Chinese Academy of Sciences(KZCX2-YW-103) ; Innovation Program of Chinese Academy of Sciences(KZCX2-YW-103) ; Institute of Geology and Geophysics, Chinese Academy of Sciences(ZC0903) ; Institute of Geology and Geophysics, Chinese Academy of Sciences(ZC0903) ; Institute of Geology and Geophysics, Chinese Academy of Sciences(ZC0903) ; Institute of Geology and Geophysics, Chinese Academy of Sciences(ZC0903) ; 40873008) ; 40873008) ; 40873008) ; 40873008) ; Natural Science Foundation of China(40773008 ; Natural Science Foundation of China(40773008 ; Natural Science Foundation of China(40773008 ; Natural Science Foundation of China(40773008 ; Innovation Program of Chinese Academy of Sciences(KZCX2-YW-103) ; Innovation Program of Chinese Academy of Sciences(KZCX2-YW-103) ; Innovation Program of Chinese Academy of Sciences(KZCX2-YW-103) ; Innovation Program of Chinese Academy of Sciences(KZCX2-YW-103) ; Institute of Geology and Geophysics, Chinese Academy of Sciences(ZC0903) ; Institute of Geology and Geophysics, Chinese Academy of Sciences(ZC0903) ; Institute of Geology and Geophysics, Chinese Academy of Sciences(ZC0903) ; Institute of Geology and Geophysics, Chinese Academy of Sciences(ZC0903) ; 40873008) ; 40873008) ; 40873008) ; 40873008) ; Natural Science Foundation of China(40773008 ; Natural Science Foundation of China(40773008 ; Natural Science Foundation of China(40773008 ; Natural Science Foundation of China(40773008 ; Innovation Program of Chinese Academy of Sciences(KZCX2-YW-103) ; Innovation Program of Chinese Academy of Sciences(KZCX2-YW-103) ; Innovation Program of Chinese Academy of Sciences(KZCX2-YW-103) ; Innovation Program of Chinese Academy of Sciences(KZCX2-YW-103) ; Institute of Geology and Geophysics, Chinese Academy of Sciences(ZC0903) ; Institute of Geology and Geophysics, Chinese Academy of Sciences(ZC0903) ; Institute of Geology and Geophysics, Chinese Academy of Sciences(ZC0903) ; Institute of Geology and Geophysics, Chinese Academy of Sciences(ZC0903) ; 40873008) ; 40873008) ; 40873008) ; 40873008) |
内容类型 | 期刊论文 |
源URL | [http://ir.iggcas.ac.cn/handle/132A11/72240] ![]() |
专题 | 中国科学院地质与地球物理研究所 |
通讯作者 | Yang, Yue-heng |
作者单位 | 1.Chinese Acad Sci, Inst Geol & Geophys, State Key Lab Lithospher Evolut, Beijing 100029, Peoples R China 2.Chinese Acad Sci, Inst Geol & Geophys, Lab Radiogen Isotope Geochem, Beijing 100029, Peoples R China |
推荐引用方式 GB/T 7714 | Yang, Yue-heng,Zhang, Hong-fu,Chu, Zhu-yin,et al. Combined chemical separation of Lu, Hf, Rb, Sr, Sm and Nd from a single rock digest and precise and accurate isotope determinations of Lu-Hf, Rb-Sr and Sm-Nd isotope systems using Multi-Collector ICP-MS and TIMS[J]. INTERNATIONAL JOURNAL OF MASS SPECTROMETRY,2010,290(2-3):120-126. |
APA | Yang, Yue-heng,Zhang, Hong-fu,Chu, Zhu-yin,Xie, Lie-wen,&Wu, Fu-yuan.(2010).Combined chemical separation of Lu, Hf, Rb, Sr, Sm and Nd from a single rock digest and precise and accurate isotope determinations of Lu-Hf, Rb-Sr and Sm-Nd isotope systems using Multi-Collector ICP-MS and TIMS.INTERNATIONAL JOURNAL OF MASS SPECTROMETRY,290(2-3),120-126. |
MLA | Yang, Yue-heng,et al."Combined chemical separation of Lu, Hf, Rb, Sr, Sm and Nd from a single rock digest and precise and accurate isotope determinations of Lu-Hf, Rb-Sr and Sm-Nd isotope systems using Multi-Collector ICP-MS and TIMS".INTERNATIONAL JOURNAL OF MASS SPECTROMETRY 290.2-3(2010):120-126. |
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