Rapid synthesis of transition metal dichalcogenide few-layer thin crystals by the microwave-induced-plasma assisted method
Chaturvedi, Apoorva1; Slabon, Adam2; Hu, Peng1; Feng, Shuanglong3; Zhang, Ke-ke1; Prabhakar, Rajiv Ramanujam1; Kloc, Christian1
刊名JOURNAL OF CRYSTAL GROWTH
2016-09-15
卷号450页码:140-147
关键词Plasma Synthesis Nanomaterials Semiconducting Materials Transition Metal Dichalcogenides
ISSN号0022-0248
DOI10.1016/j.jcrysgro.2016.06.009
英文摘要

Few-layer thin crystals of WS2, MoS2, WSe2, MoSe2 and ReS2 were synthesized via the microwave induced-plasma-assisted method. The synthesis was accomplished in plasma that was formed inside sealed quartz ampoules heated by plasma surrounding the sealed ampoule. Powder X-ray diffraction, Raman spectroscopy and Transmission Electron Microscopy indicate thin crystals of high-quality. The proposed method is rapid, reproducible and environmentally friendly. It is applicable to practically every direct reaction between metals and nonmetals if the nonmetal vapor pressure can reach a pressure of a few torr, which is required for plasma formation inside a sealed ampoule. (C) 2016 The Authors. Published by Elsevier B.V. This is an open access article under the CC BY license (hap://creativecommons.orgilicerises/by/4.0/).

资助项目Singapore National Research Foundation under its Campus for Research Excellence and Technological Enterprise (CREATE) program ; National Research Foundation, Prime Minister's Office, Singapore
WOS研究方向Crystallography ; Materials Science ; Physics
语种英语
出版者ELSEVIER SCIENCE BV
WOS记录号WOS:000382256900019
内容类型期刊论文
源URL[http://119.78.100.138/handle/2HOD01W0/2737]  
专题微纳制造与系统集成研究中心
作者单位1.Nanyang Technol Univ, Sch Mat Sci & Engn, Singapore 639798, Singapore
2.Rhein Westfal TH Aachen, Inst Inorgan Chem, D-52074 Aachen, Germany
3.Chinese Acad Sci, Chongqing Inst Green & Intelligent Technol, Chongqing 400714, Peoples R China
推荐引用方式
GB/T 7714
Chaturvedi, Apoorva,Slabon, Adam,Hu, Peng,et al. Rapid synthesis of transition metal dichalcogenide few-layer thin crystals by the microwave-induced-plasma assisted method[J]. JOURNAL OF CRYSTAL GROWTH,2016,450:140-147.
APA Chaturvedi, Apoorva.,Slabon, Adam.,Hu, Peng.,Feng, Shuanglong.,Zhang, Ke-ke.,...&Kloc, Christian.(2016).Rapid synthesis of transition metal dichalcogenide few-layer thin crystals by the microwave-induced-plasma assisted method.JOURNAL OF CRYSTAL GROWTH,450,140-147.
MLA Chaturvedi, Apoorva,et al."Rapid synthesis of transition metal dichalcogenide few-layer thin crystals by the microwave-induced-plasma assisted method".JOURNAL OF CRYSTAL GROWTH 450(2016):140-147.
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