Fabrication and characterization of He-charged ODS-FeCrNi films deposited by a radio-frequency plasma magnetron sputtering technique
Song, Liang1; Wang, Xianping1; Wang, Le1,2; Zhang, Ying1,2; Liu, Wang1; Jiang, Weibing1; Zhang, Tao1; Fang, Qianfeng1; Liu, Changsong1
刊名PLASMA SCIENCE & TECHNOLOGY
2017-04-01
卷号19期号:4页码:1-8
关键词Radio-frequency Plasma Magnetron Sputtering He-charged Fecrni-based Film Nanoindentation Hardness Elastic Recoil Detection He Implantation
DOI10.1088/2058-6272/aa57f0
文献子类Article
英文摘要He-charged oxide dispersion strengthened (ODS) FeCrNi films were prepared by a radio-frequency (RF) plasma magnetron sputtering method in a He and Ar mixed atmosphere at 150 degrees C. As a comparison, He-charged FeCrNi films were also fabricated at the same conditions through direct current (DC) plasma magnetron sputtering. The doping of He atoms and Y2O3 in the FeCrNi films was realized by the high backscattered rate of He ions and Y2O3/FeCrNi composite target sputtering method, respectively. Inductive coupled plasma (ICP) and x-ray photoelectron spectroscopy (XPS) analysis confirmed the existence of Y2O3 in FeCrNi films, and Y2O3 content hardly changed with sputtering He/Ar ratio. Cross-sectional scanning electron microscopy (SEM) shows that the FeCrNi films were composed of dense columnar nanocrystallines and the thickness of the films was obviously dependent on He/Ar ratio. Nanoindentation measurements revealed that the FeCrNi films fabricated through DC/RF plasma magnetron sputtering methods exhibited similar hardness values at each He/Ar ratio, while the dispersion of Y2O3 apparently increased the hardness of the films. Elastic recoil detection (ERD) showed that DC/RF magnetron sputtered FeCrNi films contained similar He amounts (similar to 17 at.%). Compared with the minimal change of He level with depth in DC-sputtered films, the He amount decreases gradually in depth in the RF-sputtered films. The Y2O3-doped FeCrNi films were shown to exhibit much smaller amounts of He owing to the lower backscattering possibility of Y2O3 and the inhibition effect of nano-sized Y2O3 particles on the He element.
WOS关键词FERRITIC ALLOY ; TITANIUM FILMS ; HELIUM ; MICROSTRUCTURE ; STEEL ; PARTICLES ; TENSILE
WOS研究方向Physics
语种英语
WOS记录号WOS:000398146600010
资助机构National Natural Science Foundation of China(11374299) ; National Natural Science Foundation of China(11374299) ; National Natural Science Foundation of China(11374299) ; National Natural Science Foundation of China(11374299) ; National Natural Science Foundation of China(11374299) ; National Natural Science Foundation of China(11374299) ; National Natural Science Foundation of China(11374299) ; National Natural Science Foundation of China(11374299)
内容类型期刊论文
源URL[http://ir.hfcas.ac.cn:8080/handle/334002/32956]  
专题合肥物质科学研究院_中科院固体物理研究所
作者单位1.Chinese Acad Sci, Inst Solid State Phys, Key Lab Mat Phys, Hefei 230031, Peoples R China
2.Univ Sci & Technol China, Hefei 230026, Peoples R China
推荐引用方式
GB/T 7714
Song, Liang,Wang, Xianping,Wang, Le,et al. Fabrication and characterization of He-charged ODS-FeCrNi films deposited by a radio-frequency plasma magnetron sputtering technique[J]. PLASMA SCIENCE & TECHNOLOGY,2017,19(4):1-8.
APA Song, Liang.,Wang, Xianping.,Wang, Le.,Zhang, Ying.,Liu, Wang.,...&Liu, Changsong.(2017).Fabrication and characterization of He-charged ODS-FeCrNi films deposited by a radio-frequency plasma magnetron sputtering technique.PLASMA SCIENCE & TECHNOLOGY,19(4),1-8.
MLA Song, Liang,et al."Fabrication and characterization of He-charged ODS-FeCrNi films deposited by a radio-frequency plasma magnetron sputtering technique".PLASMA SCIENCE & TECHNOLOGY 19.4(2017):1-8.
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