Two-step-method extraction of endohedral metallofullerenes | |
Hao CY ; Liu ZY ; Xu WG ; Guo XH ; Liu SY | |
刊名 | chemical journal of chinese universities-chinese
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1996 | |
卷号 | 17期号:12页码:1837-1839 |
关键词 | LAC82 EPR |
ISSN号 | 0251-0790 |
中文摘要 | a new and efficient extraction method of endohedral metallofullerenes, especially of rare-earth elements encapsulated metallofullerenes, has been reported in this paper. soxhlet-extraction of raw soot with toluene was used in the first step to wash away most accompanying c-60, c-70. then pyridine was chosen as solvent to obtain high-temperature and high pressure extract. two kinds of extract were analysed by dei-ms and ldi-ms, the results indicate that this two-step method can provide the extract which has the highest fraction of endohedral metallofullerenes. so it will greatly simplify the following separation and purification processes of metallofullerenes. |
收录类别 | SCI收录期刊论文 |
语种 | 中文 |
公开日期 | 2010-12-22 ; 2011-06-09 |
内容类型 | 期刊论文 |
源URL | [http://ir.ciac.jl.cn/handle/322003/25111] ![]() |
专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
推荐引用方式 GB/T 7714 | Hao CY,Liu ZY,Xu WG,et al. Two-step-method extraction of endohedral metallofullerenes[J]. chemical journal of chinese universities-chinese,1996,17(12):1837-1839. |
APA | Hao CY,Liu ZY,Xu WG,Guo XH,&Liu SY.(1996).Two-step-method extraction of endohedral metallofullerenes.chemical journal of chinese universities-chinese,17(12),1837-1839. |
MLA | Hao CY,et al."Two-step-method extraction of endohedral metallofullerenes".chemical journal of chinese universities-chinese 17.12(1996):1837-1839. |
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