Feasibility of Ultrafast Intermolecular Single-Quantum Coherence Spectroscopy in Analysis of Viscous-Liquid Foods | |
Cai, Hong-Hao ; Chen, Hao ; Lin, Yu-Lan ; Feng, Jiang-Hua ; Cui, Xiao-Hong ; Chen, Zhong ; Lin YL(林玉兰) ; Feng JH(冯江华) ; Cui XH(崔晓红) ; Chen Z(陈忠) | |
刊名 | http://dx.doi.org/10.1007/s12161-014-0046-x
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2014 | |
关键词 | Encoding (symbols) Magic angle spinning Mergers and acquisitions Nuclear magnetic resonance spectroscopy Quality control Quantum theory Spectrum analysis |
英文摘要 | A newly developed nuclear magnetic resonance (NMR) technique, ultrafast intermolecular single-quantum coherence (UF iSQC) spectroscopy, demonstrated its potentials to obtain spectra of viscous-liquid samples in deuterium-free environment. UF iSQC not only inherits the advantage of ultrafast acquisition efficiency of spatial encoding but also keeps the intrinsic merit of immunity of iSQC in inhomogeneous magnetic field. In the present study, UF iSQC spectroscopy is used for the direct analysis of three typical viscous-liquid foods, namely, honey, yogurt, and tomato sauce, and its feasibility is verified by ultrafast acquisition of NMR spectra of these viscous-liquid foods. UF iSQC spectroscopy presents an advantageous alternative to directly detect most components of these samples in favorable spectral information within 1 min, thus saving the trouble of complicated sample pretreatments and tedious shimming processes. Due to the immunity to field inhomogeneity, the UF iSQC technique can be a proper supplement to dilution, extraction NMR, and magic angle spinning. In addition, in comparison with the conventional iSQC method, the acquisition time of the proposed method is greatly reduced due to the introduction of the spatial encoding technique. The lower sensitivity and resolution of UF iSOC spectra than those of dilutions acquired by the conventional NMR method could be improved by some newly developed strategies. Results obtained here demonstrate the potential application of the UF iSQC spectroscopy in the quality control of food. |
语种 | 英语 |
出版者 | Springer New York LLC |
内容类型 | 期刊论文 |
源URL | [http://dspace.xmu.edu.cn/handle/2288/92240] ![]() |
专题 | 物理技术-已发表论文 |
推荐引用方式 GB/T 7714 | Cai, Hong-Hao,Chen, Hao,Lin, Yu-Lan,et al. Feasibility of Ultrafast Intermolecular Single-Quantum Coherence Spectroscopy in Analysis of Viscous-Liquid Foods[J]. http://dx.doi.org/10.1007/s12161-014-0046-x,2014. |
APA | Cai, Hong-Hao.,Chen, Hao.,Lin, Yu-Lan.,Feng, Jiang-Hua.,Cui, Xiao-Hong.,...&陈忠.(2014).Feasibility of Ultrafast Intermolecular Single-Quantum Coherence Spectroscopy in Analysis of Viscous-Liquid Foods.http://dx.doi.org/10.1007/s12161-014-0046-x. |
MLA | Cai, Hong-Hao,et al."Feasibility of Ultrafast Intermolecular Single-Quantum Coherence Spectroscopy in Analysis of Viscous-Liquid Foods".http://dx.doi.org/10.1007/s12161-014-0046-x (2014). |
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