| 气相色谱法测定甘油与盐酸反应过程的混合物; Determination of the mixture in a reaction of glycerol with hydrochloric acid by gas chromatography | |
| 尤小姿 ; 李华荣 ; 罗正鸿 | |
| 2009 | |
| 关键词 | 气相色谱 内标法 甘油 3-氯-1 2-丙二醇 1 3二氯-1-丙醇 Gas chromatography Internal standard analysis method Glycerol 3-chloro-1 2-propandiol 1 3-dichloropropanol-2-propanol |
| 英文摘要 | 采用气相色谱方法分析了甘油与盐酸反应过程中的主要物质。使用kb-WAX毛细管柱及fId检测器,以乙二醇作内标和甲醇定容,并用内标法计算。结果表明,在程序升温下,气相色谱内标法能使gly,dCP,CPd等几种物质达到基线分离,该方法能满足测试要求。; In this paper,a simple gas chromatographic method for the identification of glycerol(GLY),1,3-dichloropropanol-2-propanol,(DCP) and 3-chloro-1,2-propandiol(CPD) in GLY chlorination reaction is described.The results are detected by KB-WAX capillary column with a flame ionization detector(FID) and calculated by an internal stand method.Glycol is used as an internal standard,and the samples are diluted with methanol.This method is simple,rapid and the results are reliable. |
| 语种 | zh_CN |
| 内容类型 | 期刊论文 |
| 源URL | [http://dspace.xmu.edu.cn/handle/2288/106231]  |
| 专题 | 化学化工－已发表论文 |
| 推荐引用方式 GB/T 7714 | 尤小姿,李华荣,罗正鸿. 气相色谱法测定甘油与盐酸反应过程的混合物, Determination of the mixture in a reaction of glycerol with hydrochloric acid by gas chromatography[J],2009. |
| APA | 尤小姿,李华荣,&罗正鸿.(2009).气相色谱法测定甘油与盐酸反应过程的混合物.. |
| MLA | 尤小姿,et al."气相色谱法测定甘油与盐酸反应过程的混合物".(2009). |
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