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(1S,3S,4S)-tert-butyl N- 1-benzyl-3-hydroxy-5-phenyl-4-(picolinamido)pentyl carbamate
Zheng, J. F. ; Huang, S. Y. ; Guo, J. N. ; Zhang, Y. ; Jin, L. R. ; Zheng JF(郑剑峰)
刊名http://dx.doi.org/10.1107/S1600536808018965
2008-07
英文摘要The title compound, C29H35N3O4, was obtained by the reaction of (2S,4S,5S)-tert-butyl N-(4-amino-1-benzyl-3-hydroxy-5-phenylpentyl)carbamate and picolinic acid using oxalyl chloride as a chlorinating reagent to activate the carboxyl group. In the crystal structure there are two molecules in the asymmetric unit, which are aligned edge-to-face. In one molecule, the pyridyl ring forms a dihedral angle of 22.0 (1)degrees with the phenyl ring of the terminal benzyl group and 14.3 (1)degrees with the other phenyl ring; in the other molecule, the corresponding angles are 12.1 (1) and 10.6 (1)degrees, respectively. The packing is stabilized by intermolecular hydrogen bonds and C-H center dot center dot center dot pi interactions.
语种英语
内容类型期刊论文
源URL[http://dspace.xmu.edu.cn/handle/2288/64002]  
专题化学化工-已发表论文
推荐引用方式
GB/T 7714
Zheng, J. F.,Huang, S. Y.,Guo, J. N.,et al. (1S,3S,4S)-tert-butyl N- 1-benzyl-3-hydroxy-5-phenyl-4-(picolinamido)pentyl carbamate[J]. http://dx.doi.org/10.1107/S1600536808018965,2008.
APA Zheng, J. F.,Huang, S. Y.,Guo, J. N.,Zhang, Y.,Jin, L. R.,&郑剑峰.(2008).(1S,3S,4S)-tert-butyl N- 1-benzyl-3-hydroxy-5-phenyl-4-(picolinamido)pentyl carbamate.http://dx.doi.org/10.1107/S1600536808018965.
MLA Zheng, J. F.,et al."(1S,3S,4S)-tert-butyl N- 1-benzyl-3-hydroxy-5-phenyl-4-(picolinamido)pentyl carbamate".http://dx.doi.org/10.1107/S1600536808018965 (2008).
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