Synthesis and Crystal Structure Analysis of 5 '-O-Tosyl-2,3 '-anhydrothymidine | |
Zhao, X. E. ; Shang, P. H. ; Cheng, C. M. ; Chen, L. Q. ; Wang, R. J. ; Zhao, Y. F. ; Zhao YF(赵玉芬) | |
2013-12-12 | |
关键词 | 5 '-O-tosyl-2,3 '-anhydrothymidine synthesis X-ray diffraction crystal structure |
英文摘要 | In this paper, 5'-O-tosyl-2,3'-anhydrothymidine has been synthesized and its crystal structure was analyzed. The crystal belongs to the triclinic system, space group P1, with a = 5.397(2), b = 6.1886(18), c = 3.507(5) angstrom, alpha = 87.74(2), beta.= 89.84(4), gamma. = 73.79(2)degrees, C17H18N2O6S, M-r = 378.39, Z = 1, V = 432.8(3) angstrom(3), D-c = 1.452 g/cm(3), F(000) = 198 and Flack = -0.11(14). No intermolecular hydrogen bonds exist in the crystal, and the angle between benzene ring and pyrimidine planes is 32.23 degrees. |
语种 | 英语 |
内容类型 | 期刊论文 |
源URL | [http://dspace.xmu.edu.cn/handle/2288/63574] ![]() |
专题 | 化学化工-已发表论文 |
推荐引用方式 GB/T 7714 | Zhao, X. E.,Shang, P. H.,Cheng, C. M.,et al. Synthesis and Crystal Structure Analysis of 5 '-O-Tosyl-2,3 '-anhydrothymidine[J],2013. |
APA | Zhao, X. E..,Shang, P. H..,Cheng, C. M..,Chen, L. Q..,Wang, R. J..,...&赵玉芬.(2013).Synthesis and Crystal Structure Analysis of 5 '-O-Tosyl-2,3 '-anhydrothymidine.. |
MLA | Zhao, X. E.,et al."Synthesis and Crystal Structure Analysis of 5 '-O-Tosyl-2,3 '-anhydrothymidine".(2013). |
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