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Reversed Flow Injection Analysis of Nitrate in Drinking Water with UV-induced Reduction to Nitrite and Spectrophotometric Detection
Zhang Min ; Yuan Dong-Xing ; Feng Si-Chao ; Huang Yong-Ming ; Yuan DX(袁东星)
刊名http://dx.doi.org/10.3724/SP.J.1096.2011.00943
2011-06
关键词Nitrate ultraviolet-induced reduction Flow injection Spectrophotometry
英文摘要An environmental friendly method was developed based on reversed flow injection (r-FIA) with UV-induced reduction of nitrate to nitrite and spectrophotometric detection. Sample or standard solutions were mixed with a phosphate buffer solution containing diethylenetriaminepentaacetate (DTPA), and then passed through a UV reduction reactor equipped with an 8 W low pressure mercury lamp, where the nitrate was reduced to nitrite. The formed nitrite was detected with spectrophotometric method through Griess reaction. Less than 20 mu mol/L of nitrite showed no effect on the nitrate analysis. Reduction efficiency over 80% was obtained. The detection limit of the proposed method was 0. 053 mu mol/L and linear range was 0. 2-40 mu mol/L. A sample of 20 mu mol/L nitrate was continually measured for 48 times, and a RSD of 2. 22% was obtained. The recoveries of drinking waters were between 90. 9%-100. 6%.
语种英语
内容类型期刊论文
源URL[http://dspace.xmu.edu.cn/handle/2288/60733]  
专题海洋环境-已发表论文
推荐引用方式
GB/T 7714
Zhang Min,Yuan Dong-Xing,Feng Si-Chao,et al. Reversed Flow Injection Analysis of Nitrate in Drinking Water with UV-induced Reduction to Nitrite and Spectrophotometric Detection[J]. http://dx.doi.org/10.3724/SP.J.1096.2011.00943,2011.
APA Zhang Min,Yuan Dong-Xing,Feng Si-Chao,Huang Yong-Ming,&袁东星.(2011).Reversed Flow Injection Analysis of Nitrate in Drinking Water with UV-induced Reduction to Nitrite and Spectrophotometric Detection.http://dx.doi.org/10.3724/SP.J.1096.2011.00943.
MLA Zhang Min,et al."Reversed Flow Injection Analysis of Nitrate in Drinking Water with UV-induced Reduction to Nitrite and Spectrophotometric Detection".http://dx.doi.org/10.3724/SP.J.1096.2011.00943 (2011).
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