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Study of thermal perturbation of natural bamboo fiber by two dimensional correlation analysis and Fourier transform infrared spectroscopy
Huang An-min ; Wang Ge ; Zhou Qun ; Liu Jun-liang ; Sun Su-qin
2010-10-12 ; 2010-10-12
关键词Experimental/ chemical analysis Fourier transform spectroscopy heating natural fibres oxidation/ natural bamboo fiber dimensional correlation analysis Fourier transform infrared spectroscopy thermal perturbation miniheating process FTIR spectra chemical composition oxidation mechanism temperature 50 C to 120 C/ E3614 Wood processing industry E1710 Engineering materials E1525 Industrial processes E1640 Instrumentation/ temperature 3.2315E+02 to 3.9315E+02 K
中文摘要The Fourier transform infrared spectroscopy (FTIR) combined with generalized two-dimensional correlation analysis was applied to study the mini-heating process of natural bamboo fiber. The absorption peaks of natural bamboo fiber and bamboo in the FTIR spectra were different, which showed the contents of lignin and hemicelluloses of natural bamboo fiber was lower than those of bamboo. The changes in absorption peaks of natural bamboo fiber in the FTIR spectra at different temperatures were inconspicuous during heating up from 50 to 120 degrees C , which showed that there was not oxidation reaction in natural bamboo fiber during the process. With the help of 2D correlation analysis, the changes of different groups of natural bamboo fiber and bamboo during heating process were reflected. The strongest autopeak of them was all aroused at 1665 cm/sup -1/ in synchronous spectrum. The difference was that there were several weak auto-peaks and cross peaks in the natural bamboo fiber, but in the bamboo, one stronger 5*5 group was aroused in the 833-1 230 cm/sup -1/. Region the reason was the difference in chemistry composition and the change degree during heating process. In conclusion, the 2D correlation analysis of FTIR can be a new method to analyze the microcosmic dynamic change in the structure of natural bamboo fiber and bamboo during the mini-heating process and also offers an important theory gist for the study of oxidation mechanism of them.
语种中文
出版者Editorial Board of Spectroscopy and Spectral Analysis ; China
内容类型期刊论文
源URL[http://hdl.handle.net/123456789/80956]  
专题清华大学
推荐引用方式
GB/T 7714
Huang An-min,Wang Ge,Zhou Qun,et al. Study of thermal perturbation of natural bamboo fiber by two dimensional correlation analysis and Fourier transform infrared spectroscopy[J],2010, 2010.
APA Huang An-min,Wang Ge,Zhou Qun,Liu Jun-liang,&Sun Su-qin.(2010).Study of thermal perturbation of natural bamboo fiber by two dimensional correlation analysis and Fourier transform infrared spectroscopy..
MLA Huang An-min,et al."Study of thermal perturbation of natural bamboo fiber by two dimensional correlation analysis and Fourier transform infrared spectroscopy".(2010).
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