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	利用凝胶层析分离测定胶体态铝和溶解态铝的研究
	赵华章 ; 杨宏伟 ; 蒋展鹏 ; 师绍琪 ; ZHAO Huazhang ; YANG Hongwei ; JIANG Zhanpeng ; SHI Shaoqi
	2010-06-10 ; 2010-06-10
关键词	凝胶层析 胶体态铝 溶解态铝 分离测定 gel chromatography colloidal aluminum soluble aluminum separation and measurement X132
其他题名	Study on the separation and determination of colloidal aluminum and soluble aluminum by gel chromatography
中文摘要	利用凝胶层析柱分别对高浓度(5.4g.L-1)和低浓度(0.27mg.L-1)的聚合氯化铝溶液和氯化铝溶液进行了层析分离,测定了洗脱流出液的电导率和pH值,并采用Al-Ferron逐时络合比色分析了洗脱流出液中的铝形态分布.结果表明,高浓度和低浓度铝水样中的胶体态铝和溶解态铝浓度均可采用凝胶层析法进行分离测定.利用凝胶层析装置对2.5mL铝水样以1mL.min-1的速度进行洗脱,40~60mL间的洗脱流出液即为胶体态铝,剩余部分为溶解态铝.; The polyaluminum chloride (PAC) solution and aluminum chloride solution with high (5.4g稬~ -1 ) and low (0.27mg稬~ -1 ) Al concentrations were chromatographed by gel-filtration column, respectively. The conductivity and pH value of the eluted fractions were measured and the aluminium species distribution of the eluted fractions was also analyzed by Ferron assay. The experimental results show that the separation and determination of colloidal aluminum and soluble aluminum in the water samples with high or low Al content can be achieved by gel chromatography. Under the condition that 2.5mL of the studied sample is eluted at a rate of 1 mL穖in~ -1 with the gel-filtration device, the eluted fraction from 40mL to 60mL corresponds to the colloidal aluminum and the rest part corresponds to the soluble aluminum. The concentrations of the colloidal aluminum and the soluble aluminum can be achieved by measurement with inductively coupled plasma (ICP) spectrometer plus further conversion.; 国家自然科学基金重点资助项目(No.50238020)~~
语种	中文 ; 中文
内容类型	期刊论文
源URL	[http://hdl.handle.net/123456789/64753]
专题	清华大学
推荐引用方式 GB/T 7714	赵华章,杨宏伟,蒋展鹏,等. 利用凝胶层析分离测定胶体态铝和溶解态铝的研究[J],2010, 2010.
APA	赵华章.,杨宏伟.,蒋展鹏.,师绍琪.,ZHAO Huazhang.,...&SHI Shaoqi.(2010).利用凝胶层析分离测定胶体态铝和溶解态铝的研究..
MLA	赵华章,et al."利用凝胶层析分离测定胶体态铝和溶解态铝的研究".(2010).

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