丹皮药材的高效液相色谱-质谱/质谱研究 | |
梁琼麟 ; 温华珍 ; 王玉莉 ; 罗国安 ; 王义明 ; Liang Qionglin ; Wen Huazhen ; Wang Yuli ; Luo Guoan ; Wang Yiming | |
2010-06-10 ; 2010-06-10 | |
关键词 | 丹皮 高效液相色谱-质谱/质谱 指纹图谱 Cortex Moutan,high performance liquid chromatography tandem mass spectrometric,fingerprint O657.63 TQ461 |
其他题名 | Investigation of Cortex Moutan by Liquid Chromatography Coupling with Tandem Mass Spectrometry |
中文摘要 | 采用高效液相色谱-质谱/质谱建立了丹皮药材的指纹图谱方法。丹皮药材中的主要成分得到较好分离,指纹峰重现性好,通过多维联用技术获得各指纹峰的保留时间、分子量及结构信息,推测出15个指纹峰的可能组成。结果表明:所建立的丹皮指纹图谱信息量丰富,对丹皮药材的化学表征及质量评价有重要的参考价值。; A high performance liquid chromatography tandem mass spectrometric(HPLC/MS/MS) method was developed to establish the fingerprint of Cortex Moutan,a Chinese medicinal herb.The major constituents among Cortex Moutan from different origins were separated well by HPLC and the fingerprint had a good(repeatability).Fifteen peaks in the fingerprint were identified by LC/MS/MS according to their retention time,molecular weight and fragmentation information.The result showed that the presented fingerprint of Cortex Moutan contained plenty of information,which was quite valuable for the quality evaluation as well as chemical characterization of this Chinese herb.; 国家自然基金重点项目(No.9020905); 科技部“十五”攻关项目(No.2002BA90629-3)资助 |
语种 | 中文 ; 中文 |
内容类型 | 期刊论文 |
源URL | [http://hdl.handle.net/123456789/60997] ![]() |
专题 | 清华大学 |
推荐引用方式 GB/T 7714 | 梁琼麟,温华珍,王玉莉,等. 丹皮药材的高效液相色谱-质谱/质谱研究[J],2010, 2010. |
APA | 梁琼麟.,温华珍.,王玉莉.,罗国安.,王义明.,...&Wang Yiming.(2010).丹皮药材的高效液相色谱-质谱/质谱研究.. |
MLA | 梁琼麟,et al."丹皮药材的高效液相色谱-质谱/质谱研究".(2010). |
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