电子束辐照下呋喃西林代谢产物降解的质谱检测 | |
杨成对 ; 宋莉晖 ; 刘志涛 ; 刘密新 ; 张化一 ; YANG Cheng-dui ; SONG Li-hui ; LIU Zhi-tao ; LIU Mi-xin ; ZHANG Hua-yi | |
2010-06-10 ; 2010-06-10 | |
关键词 | 呋喃西林 氨基脲 电子束辐照 降解 液相色谱-串联质谱 Nitrofurazone Semicarbazide(SC) Electronic irradiation Degrading LC-MS/MS O657.63 TQ463.53 |
其他题名 | Mass Spectrum Detection of Nitrofurazone Metabolite′s Degraded by Electronic Beam Irradiation |
中文摘要 | 提出用电子束辐照技术降解去除水溶液中的呋喃西林代谢形成的氨基脲(SC)。采用LC-MS/MS方法分析SC含量变化。结果表明:当SC质量浓度小于0.67 mg/L、辐照强度大于8 kGy时,SC降解率高达90%以上,没有检测到明显的降解产物。可见,电子束辐照降解法是一种简便、有效的有机污染物去除方法。; Semicarbazide(SC)is a metabolite coming from nitrofurazone.It can reside in animal tissues for a long time.Both nitrofurazone and SC are classified as mutagenic and genotoxic drugs.Their residues will be harmful for the health of consumers.This paper proposes a method thatcan remove SC fromwater through elecˉtronic irradiation.Multi-reaction monitoring(MRM)scan technology of LCMS/MS was used as an analytiˉcal method for determination the SC concentration after irradiation.The results showed that electronic irradiaˉtion is a simple and efficient method for removing organic contaminations such as SC.When the SC concentraˉtion was less than0.67mg/L,the irradiation dosage was more than8kGy,and the degradation rate of SC was up to90%. |
语种 | 中文 ; 中文 |
内容类型 | 期刊论文 |
源URL | [http://hdl.handle.net/123456789/60969] ![]() |
专题 | 清华大学 |
推荐引用方式 GB/T 7714 | 杨成对,宋莉晖,刘志涛,等. 电子束辐照下呋喃西林代谢产物降解的质谱检测[J],2010, 2010. |
APA | 杨成对.,宋莉晖.,刘志涛.,刘密新.,张化一.,...&ZHANG Hua-yi.(2010).电子束辐照下呋喃西林代谢产物降解的质谱检测.. |
MLA | 杨成对,et al."电子束辐照下呋喃西林代谢产物降解的质谱检测".(2010). |
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