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Synthesis of BiFeO/sub 3/-PbTiO/sub 3/ powders by sol-gel auto-combustion process
Hao Sheng ; Zhenxing Yue ; Zhilun Gui ; Longtu Li
2010-05-10 ; 2010-05-10
会议名称Key Engineering Materials ; 3rd International Conference on High-Performance Ceramics (CICC-3) ; Shenzhen, China ; INSPEC
关键词Experimental/ bismuth compounds combustion synthesis differential thermal analysis infrared spectra lead compounds oxidation powder technology reduction (chemical) scanning electron microscopy sol-gel processing thermal analysis X-ray diffraction/ BiFeO/sub 3/-PbTiO/sub 3/ powders autocombustion process sol-gel method metal nitrate citric acid self-propagating combustion process voluminous ashes single phase perovskite redox properties DTA thermogravimetry IR spectra XRD SEM BiFeO/sub 3/-PbTiO/sub 3// A8120L Preparation of ceramics and refractories A8120E Powder techniques, compaction and sintering A7830G Infrared and Raman spectra in inorganic crystals A8230 Specific chemical reactions reaction mechanisms/ BiFeO3PbTiO3/ss FeO3/ss TiO3/ss Bi/ss Fe/ss O3/ss Pb/ss Ti/ss O/ss
中文摘要BiFeO/sub 3/-PbTiO/sub 3/ powders were synthesized by a novel sol-gel auto-combustion method. The gels, transformed from the aqueous solutions of metal nitrate and citric acid, undergo a self-propagating combustion process when being ignited and yield voluminous ashes. These ashes are single phase perovskite BiFeO/sub 3 /-PbTiO/sub 3/ powders. The redox behaviors of the dried gels were studied by DTA-TG technique and IR spectra. The synthesized powders were characterized in terms of XRD, SEM and BET techniques.
会议录出版者Trans Tech Publications ; Switzerland
语种英语 ; 英语
内容类型会议论文
源URL[http://hdl.handle.net/123456789/18159]  
专题清华大学
推荐引用方式
GB/T 7714
Hao Sheng,Zhenxing Yue,Zhilun Gui,et al. Synthesis of BiFeO/sub 3/-PbTiO/sub 3/ powders by sol-gel auto-combustion process[C]. 见:Key Engineering Materials, 3rd International Conference on High-Performance Ceramics (CICC-3), Shenzhen, China, INSPEC.
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