Comparison of the performance of microemulsion electrokinetic chromatography and 1-butanol modified micellar electrokinetic chromatography on the separations of amphetamine and it's ephedra alkaloid impurities | |
Wen Tao ; Zhao Xia ; Luo Guoan ; Wang Yiming ; Wang Jian ; Zhu Jun ; Yu Zhongshan | |
2010-05-06 ; 2010-05-06 | |
关键词 | amphetamine ephedrine microemulsion electrokinetic chromatography micellar electrokinetic chromatography separation CAPILLARY CHROMATOGRAPHY SELECTIVITY HEROIN Chemistry, Analytical |
中文摘要 | Simultaneous separation of 9 species of amphetamines and their basic ephedra alkaloid impurities was conducted within 10 minutes by capillary microemulsion electrokinetic chromatography. Meanwhile, the separation performance of microemulsion elec,trokinetic chromatography was compared with the separation by micellar electrokinetic chromatography with 1-butanol as modifier, and the influences of pH and 1-butanol cosurfactant on the separations were investigated, and 1-butanol was found to be a principal factor to improve separation efficiency in the two separation modes. The developed microemulsion electrokinetic chromatographic method for separation of amphetamine is stable, and the RSDs for relative migration time and relative peak area are less than 1. 3% and 5. 0% respectively, so it can be applied in the analysis and determination of practical amphetamine samples. |
语种 | 中文 ; 中文 |
出版者 | SCIENCE CHINA PRESS ; BEIJING ; 16 DONGHUANGCHENGGEN NORTH ST, BEIJING 100717, PEOPLES R CHINA |
内容类型 | 期刊论文 |
源URL | [http://hdl.handle.net/123456789/12976] |
专题 | 清华大学 |
推荐引用方式 GB/T 7714 | Wen Tao,Zhao Xia,Luo Guoan,et al. Comparison of the performance of microemulsion electrokinetic chromatography and 1-butanol modified micellar electrokinetic chromatography on the separations of amphetamine and it's ephedra alkaloid impurities[J],2010, 2010. |
APA | Wen Tao.,Zhao Xia.,Luo Guoan.,Wang Yiming.,Wang Jian.,...&Yu Zhongshan.(2010).Comparison of the performance of microemulsion electrokinetic chromatography and 1-butanol modified micellar electrokinetic chromatography on the separations of amphetamine and it's ephedra alkaloid impurities.. |
MLA | Wen Tao,et al."Comparison of the performance of microemulsion electrokinetic chromatography and 1-butanol modified micellar electrokinetic chromatography on the separations of amphetamine and it's ephedra alkaloid impurities".(2010). |
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