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	Synthesis of N-phosphoryl branched peptides
	Yang, J ; Jiang, YY ; Cao, SL ; Fu, H ; Zhao, YF
	2010-05-06 ; 2010-05-06
关键词	N-phosphoryl branched peptide H-phosphonate Atherton-Todd reaction transesterification Chemistry, Multidisciplinary
中文摘要	H-phosphonates were conveniently prepared by direct transesterification of diphenyl phosphite (DPP) with the corresponding alcohols, without further purification they were reacted with branched peptide methyl ester (L-Leu(2)-L-LysOMe) through Atherton-Todd method, a series of different substituted alkyloxy (N-phosphoryl-L-Leu)(2)-L-LysOMe were synthesized, and their structures were confirmed by P-31 NMR, ESI-MS, H-1 NMR, C-13 NMR, IR and elemental analysis. The approach possesses the advantages of easy operation, high yield and inexpensive phosphorylating reagent.
语种	英语 ; 英语
出版者	CHINESE CHEMICAL SOCIETY ; BEIJING ; C/O DEPT INT AFFAIRS, SECRETARY OF CHEM SOC, PO BOX 2709, BEIJING 100080, PEOPLES R CHINA
内容类型	期刊论文
源URL	[http://hdl.handle.net/123456789/12466]
专题	清华大学
推荐引用方式 GB/T 7714	Yang, J,Jiang, YY,Cao, SL,et al. Synthesis of N-phosphoryl branched peptides[J],2010, 2010.
APA	Yang, J,Jiang, YY,Cao, SL,Fu, H,&Zhao, YF.(2010).Synthesis of N-phosphoryl branched peptides..
MLA	Yang, J,et al."Synthesis of N-phosphoryl branched peptides".(2010).

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