Determination of impurities in titanium nitride by slurry introduction axial viewed inductively coupled plasma optical emission spectrometry

CORC > 生态环境研究中心 > 中国科学院生态环境研究中心 > 环境化学与生态毒理学国家重点实验室

	Determination of impurities in titanium nitride by slurry introduction axial viewed inductively coupled plasma optical emission spectrometry
	Wang, Z; Ni, ZM; Qui, DR; Tao, GY; Yang, PY
刊名	SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY
	2005
卷号	60 期号:3 页码:361-367
关键词	slurry TiN axial ICP-OES NH(4)PAA intrinsic internal standard
英文摘要	A method of slurry nebulization for inductively coupled plasma optical emission spectrometry (ICP-OES) applied to the analysis of titanium niride(TiN) was reported. The TiN slurry sample was prepared with adding dispersant polyacrylate amine or polyethylene imine for the stabilization and homogenization of suspension, and the amount of additives was optimized. A Babington type cross-flow nebulizer with V-groove was used for nebulization of the slurry for avoidance of blockage from the particles. The stability of slun-y was characterized via zeta potential measurement, scanning electron microscope observation, particle size distrbution measurement and signal stability testing. For nm size TiN, calibration curves could be established by aqueous standards and the analytical results were in good accordance with the alkaline fusion method. For μ m size TiN, a negative deviation was observed for most of elements and this deviation can be corrected by using Ti intrinsic internal standard method. © 2005 Elsevier B.V. All rights reserved.
学科主题	Spectroscopy
研究领域[WOS]	Spectroscopy
公开日期	2015-12-24
内容类型	期刊论文
源URL	[http://ir.rcees.ac.cn/handle/311016/23164]
专题	生态环境研究中心_环境化学与生态毒理学国家重点实验室
推荐引用方式 GB/T 7714	Wang, Z,Ni, ZM,Qui, DR,et al. Determination of impurities in titanium nitride by slurry introduction axial viewed inductively coupled plasma optical emission spectrometry[J]. SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY,2005,60(3):361-367.
APA	Wang, Z,Ni, ZM,Qui, DR,Tao, GY,&Yang, PY.(2005).Determination of impurities in titanium nitride by slurry introduction axial viewed inductively coupled plasma optical emission spectrometry.SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY,60(3),361-367.
MLA	Wang, Z,et al."Determination of impurities in titanium nitride by slurry introduction axial viewed inductively coupled plasma optical emission spectrometry".SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY 60.3(2005):361-367.